3-苯基-2-丙炔-1-醇合成路线 （共 165 条）
反应条件
n-butyllithium; N,N,N',N,-tetramethylethylenediamine 1) hexane, reflux, 3 h; Multistep reaction. Title compound not separated from byproducts;
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 104, # 9 p. 226 - 230
参考文献
Journal of Organometallic Chemistry, , vol. 288, p. 349 - 358
反应条件
T=700°C; various pyrazolines; Product distributionMechanism;
参考文献
Journal of the Chemical Society. Perkin Transactions 2, , # 2 p. 211 - 216
反应条件
sodium hydride 1.) THF, reflux, 2 h, 2.) THF, RT; Yield given. Multistep reaction;
参考文献
Goff, Dane A.; Harris, Ralph N.; Bottaro, Jeffrey C.; Bedford, Clifford D.
Journal of Organic Chemistry, 1986 , vol. 51, # 24 p. 4711 - 4714
反应条件
1: 3-phenyl-2-propyn-1-ol (phenyl propargyl alcohol) With n-butyllithium in tetrahydrofuran T=20°C; 0.5 h; 2: carbon dioxide in tetrahydrofuran T=0 - 20°C; 1.5 h; 3: 3-chloroprop-1-ene With dichloro bis(acetonitrile) palladium(II) in tetrahydrofuran T=20°C; 3 h;
参考文献
Maddess, Matthew L.; Lautens, Mark
Synthesis, 2004 , # 9 p. 1399 - 1408
反应条件
oxalyl dichloride; Bis-lt;(p-methoxy)phenylgt;cyclopropenon in dichloromethane T=30°C; 1 h; Inert atmosphere;
参考文献
Vanos, Christine M.; Lambert, Tristan H.
Angewandte Chemie - International Edition, 2011 , vol. 50, # 51 p. 12222 - 12226
反应条件
pyridine in (2S)-N-methyl-1-phenylpropan-2-amine hydrate
参考文献
Yoshitomi Pharmaceutical Industries, Ltd.; Taito Co., Ltd.
Patent: US5604229 A1, 1997 ;
反应条件
iodine; Poly[4-(diacetoxy)iodo]styrene T=20°C; 5 h;
参考文献
Liu, Xiao-Ling; Lin, Shu-Ying; Sheng, Shou-Ri; Wei, Mei-Hong; Gong, Bin
Journal of the Chinese Chemical Society, 2007 , vol. 54, # 5 p. 1119 - 1122
反应条件
palladium diacetate; potassium carbonate; triphenylphosphine in 1,4-dioxane T=101°C; Inert atmosphere;
参考文献
Rodriguez, Arantxa; Moran, Wesley J.
Letters in Organic Chemistry, 2010 , vol. 7, # 1 p. 7 - 10
反应条件
1.1: Et3N / CH2Cl2 / 0.5 h / 20 °C 2.1: NaH / tetrahydrofuran / 1 h / 20 °C 2.2: tetrahydrofuran / 20 °C View Scheme
参考文献
Kobayashi, Toshitake; Koga, Yuji; Narasaka, Koichi
Journal of Organometallic Chemistry, 2001 , vol. 624, # 1-2 p. 73 - 87
