(’±)-2-苯基环庚酮合成路线 （共 37 条）
反应条件
in cyclohexane Irradiation; Product distribution;
参考文献
Journal of Organic Chemistry, , vol. 64, # 11 p. 3802 - 3803
反应条件
oxygen in isopropyl alcohol 0.333333 h; UV-irradiation; Product distribution;
参考文献
Kohtani, Shigeru; Sugiyama, Masahide; Fujiwara, Yoshihisa; Tanimoto, Yoshifumi; Nakagaki, Ryoichi
Bulletin of the Chemical Society of Japan, 2002 , vol. 75, # 6 p. 1223 - 1233
反应条件
1: phenyl-magnesium chloride With AlCl3, aluminium chloride in tetrahydrofuran
2: cycloheptanone With dihydro-isoxazole in tetrahydrofuran; dichloromethane
T=0 - 20°C; regioselective reaction;
参考文献
Miyoshi, Tetsuya; Sato, Shohei; Tanaka, Hiroya; Hasegawa, Chihiro; Ueda, Masafumi; Miyata, Okiko
Tetrahedron Letters, 2012 , vol. 53, # 32 p. 4188 - 4191
反应条件
gallium(III) chloride; 2-methyl cyclohexane in 1,2-dichloro-ethane
T=80°C; 12 h;
参考文献
Oshita, Masayuki; Okazaki, Takao; Ohe, Kouichi; Chatani, Naoto
Organic Letters, 2005 , vol. 7, # 2 p. 331 - 334
反应条件
diethylzinc in dichloromethane
T=20°C; 2 h;
参考文献
Li, Lezhen; Cai, Peijie; Guo, Qingxiang; Xue, Song
Journal of Organic Chemistry, 2008 , vol. 73, # 9 p. 3516 - 3522
反应条件
1: cyclohexanone With scandium tris(trifluoromethanesulfonate) in toluene
T=20°C; 0.0833333 h; Inert atmosphere;
2: phenyldiazomethane in toluene
T=-78 - 0°C; Inert atmosphere;
参考文献
Rendina, Victor L.; Kaplan, Hilan Z.; Kingsbury, Jason S.
Synthesis, 2012 , vol. 44, # 5 p. 686 - 693
反应条件
1: With 1,1-dimethylethylmagnesium chloride in tetrahydrofuran
T=-45°C; Inert atmosphere;
2: With isopropylmagnesium chloride in tetrahydrofuran
T=-45 - 20°C; Inert atmosphere;
参考文献
Fukuda, Shigehiko; Tsuji, Kazuhito; Musashi, Jun; Nonaka, Ryo; Kimura, Tsutomu; Satoh, Tsuyoshi
Synthesis, 2011 , # 22 art. no. F71511SS, p. 3615 - 3626
反应条件
(hydroxy(tosyloxy)iodo)benzene in methanol
T=20°C; 1 h;
参考文献
Justik, Michael W.; Koser, Gerald F.
Tetrahedron Letters, 2004 , vol. 45, # 32 p. 6159 - 6163
反应条件
potassium carbonate in methanol
T=20 - 25°C;
参考文献
Wang, Xiaowei; Lou, Qinghua; Guo, Ying; Xu, Yang; Zhang, Zhili; Liu, Junyi
Organic and Biomolecular Chemistry, 2006 , vol. 4, # 17 p. 3252 - 3258
反应条件
methanol; potassium carbonate
T=25°C;
参考文献
Gutsche
Journal of the American Chemical Society, 1949 , vol. 71, p. 3513,3515
Full Text Show Details
Gutsche; Johnson
Organic Syntheses, 1963 , vol. Coll. Vol. IV, p. 780,781
