反应条件
1: 41 percent / 1-hydroxybenzotriazole hydrate, N-(N,N'-dimethylaminopropyl)-N'-ethylcarbodiimide hydrochloride, triethylamine / dimethylformamide / 1.) RT, 2 d, 2.) 50 deg C, 3 h
2: 94 percent / H2 / 5percent Pd/C / acetic acid / 2585.7 Torr / Ambient temperature
3: 92 percent / triethylamine / benzene / 5 h
View Scheme
参考文献
Fontes, Ernest; Lee, Wah Keat; Heiney, Paul A.; Nounesis, George; Garland, Carl W.; et al.
Journal of Chemical Physics, 1990 , vol. 92, # 6 p. 3917 - 3929