hydrogen; N-ethyl-N,N-diisopropylamine; [rhodium(I)(carbonyl)2(acetylacetonate)] in decane; toluene T=80°C; P=15001.5 Torr; 1 h; Further byproducts.;
参考文献
Slagt, Vincent F.; Kaiser, Patrick; Berkessel, Albrecht; Kuil, Mark; Kluwer, Alexander M.; Van Leeuwen, Piet W. N. M.; Reek, Joost N. H.
European Journal of Inorganic Chemistry, 2007 , # 29 p. 4653 - 4662
→
反应条件
sodium chloride; ethanol in 1,4-dioxane; mineral oil
potassium-sodium; tert-butyl alcohol; 18-crown-6 ether in tetrahydrofuran T=0°C; 0.5 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Mathre, David J.; Guida, Wayne C.
Tetrahedron Letters, 1980 , vol. 21, p. 4773 - 4776
