氯化三(三苯基膦)合铑(I)合成路线 （共 95 条）
反应条件
in benzene-d6 byproducts: C6H5Cl5; identified by NMR;
参考文献
Organometallics, , vol. 23, # 16 p. 3891 - 3897
反应条件
in further solvent(s) in boiling 2-methoxyethanol;
参考文献
Journal of the Chemical Society [Section] A: Inorganic, Physical, Theoretical, , p. 3322 - 3326
参考文献
Journal of the Chemical Society, Chemical Communications, , # 23 p. 1733 - 1734
反应条件
in tetrahydrofuran N2-atmosphere; stirring of stoich. amts. (room temp., 4 h); evapn. (vac.); Co-complexes not sepd., detd. by IR-spectroscopy; Rh-complex isolated by extn. (benzene);
参考文献
Inorganica Chimica Acta, , vol. 32, p. 171 - 174
反应条件
in tetrahydrofuran (Ar), Schlenk techniques; slow addn. of soln. of N compd. in THF to soln. of Rh complex in THF at room temp.;
参考文献
Organometallics, , vol. 30, # 19 p. 5208 - 5213
反应条件
byproducts: H2; identified by 31P NMR spectroscopy;
参考文献
Inorganica Chimica Acta, , vol. 146, p. 89 - 92
参考文献
Progr. Inorg. Chem., , vol. 28, p. 63 - 202
反应条件
potassium hydroxide in ethanol; water 0.166667 h; RefluxSchlenk techniqueInert atmosphere;
参考文献
Catalysis Today, , vol. 200, # 1 p. 54 - 62
反应条件
2,2,6,6-tetramethylpiperine in further solvent(s) argon-filled glovebox, bibenzyl, 130°C, 28h, further products; product detd. by GC;
参考文献
Andrews, Mark A.
Organometallics, 1989 , vol. 8, p. 2703 - 2708
反应条件
2,2,6,6-tetramethylpiperine in further solvent(s) argon-filled glovebox, bibenzyl, 130°C, 28h, further products; product detd. by GC;
参考文献
Andrews, Mark A.
Organometallics, 1989 , vol. 8, p. 2703 - 2708
