potassium iodide in dimethyl sulfoxide T=100°C; 20 h;
参考文献
Veerman, Johan J. N.; Klein, Jasper; Aben, Rene W. M.; Scheeren, Hans W.; Kruse, Chris G.; Van Maarseveen, Jan H.; Rutjes, Floris P. J. T.; Hiemstra, Henk
European Journal of Organic Chemistry, 2002 , # 18 p. 3133 - 3139
lithium aluminium tetrahydride in diethyl ether T=0°C; 3 h;
参考文献
Veerman, Johan J. N.; Klein, Jasper; Aben, Rene W. M.; Scheeren, Hans W.; Kruse, Chris G.; Van Maarseveen, Jan H.; Rutjes, Floris P. J. T.; Hiemstra, Henk
European Journal of Organic Chemistry, 2002 , # 18 p. 3133 - 3139
1: 55 percent / LiAlH4 / diethyl ether / 3 h / 0 °C
2: 87 percent / DIPEA / CH2Cl2 / 5 h / 20 °C
3: pTSA / CH2Cl2 / 20 °C
View Scheme
参考文献
Veerman, Johan J. N.; Klein, Jasper; Aben, Rene W. M.; Scheeren, Hans W.; Kruse, Chris G.; Van Maarseveen, Jan H.; Rutjes, Floris P. J. T.; Hiemstra, Henk
European Journal of Organic Chemistry, 2002 , # 18 p. 3133 - 3139
