三甲基[(2-苯基-2-丙基)氧基]硅烷合成路线 (共 12 条)
反应条件
Ammonium thiocyanate in dichloromethane T=0 - 20°C; 0.416667 h;
参考文献
Jadhav, Vrushali H.; Kumar, K. S. Ajish; Chaudhari, Vinod D.; Dhavale, Dilip D.
Synthetic Communications, 2007 , vol. 37, # 8 p. 1363 - 1370
反应条件
bis(η3-allyl-μ-chloropalladium(II)); triphenylphosphine in N,N-dimethyl acetamide T=80°C; 3 h;
参考文献
Shirakawa, Eiji; Hironaka, Koji; Otsuka, Hidehito; Hayashi, Tamio
Chemical Communications, 2006 , # 37 p. 3927 - 3929
反应条件
magnesium in N,N-dimethyl-formamide T=20°C; O-Silylation;
参考文献
Nishiguchi, Ikuzo; Kita, Yoshio; Watanabe, Masamitsu; Ishino, Yoshio; Ohno, Toshinobu; Maekawa, Hirofumi
Synlett, 2000 , # 7 p. 1025 - 1027
反应条件
tetrabutyl ammonium fluoride in tetrahydrofuran Ambient temperature;
参考文献
Johnson
Carbohydrate Research, 1992 , vol. 237, p. 313 - 318
反应条件
1 Au/TiO2 in ethyl acetate T=55°C; 1.5 h; Overall yield = 82 percent;
参考文献
Gryparis, Charis; Stratakis, Manolis
Chemical Communications (Cambridge, United Kingdom), 2012 , vol. 48, # 87 p. 10751 - 10753,3
反应条件
in tetrahydrofuran 1 h; -70 --> 25 deg C;
参考文献
Matsuzawa, Satoshi; Isaka, Masahiko; Nakamura, Eiichi; Kuwajima, Isao
Tetrahedron Letters, 1989 , vol. 30, # 15 p. 1975 - 1978
反应条件
in various solvent(s) T=343°C; E(activ.); Rate constantProduct distributionMechanism;
参考文献
Gorbatov, V. V.; Yablokova, N. V.; Aleksandrov, Yu. A.; Ivanov, V. I.
J. Gen. Chem. USSR (Engl. Transl.), 1983 , vol. 53, # 8 p. 1752 - 1755,1576 - 1578
反应条件
in various solvent(s) T=343°C; E(activ.); Rate constantMechanismProduct distribution;
参考文献
Gorbatov, V. V.; Yablokova, N. V.; Aleksandrov, Yu. A.; Ivanov, V. I.
J. Gen. Chem. USSR (Engl. Transl.), 1983 , vol. 53, # 8 p. 1752 - 1755,1576 - 1578
反应条件
multistep reaction, products isolated in the course of reaction; Product distribution;
参考文献
Musavirov, R. S.; Mullakhmetova, Z. F.; Nedogrei, E. P.; Kantor, E. A.; Rakmankulov, D. L.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1985 , vol. 21, # 11 p. 1297 - 1298
Khimiya Geterotsiklicheskikh Soedinenii, 1985 , vol. 21, # 11 p. 1571 - 1572
反应条件
potassium fluoride; tetraethylene glycol T=20°C; 20 h;
参考文献
Yan, Hailong; Oh, Joong-Suk; Song, Choong Eui
Organic and Biomolecular Chemistry, 2011 , vol. 9, # 23 p. 8119 - 8121