5,6,11,12-四氢二苯并[a,e]环辛烯合成路线 （共 46 条）
反应条件
48 h; Ambient temperature;
参考文献
Errede,L.A.
Journal of Organic Chemistry, 1961 , vol. 26, p. 2606 - 2608
参考文献
Jensen; Coleman
Tetrahedron Letters, 1959 , # 20 p. 7,10
参考文献
Baker et al.
Journal of the Chemical Society, 1945 , p. 27,29
反应条件
1: CCl4; N-bromo-succinimide
2: quinoline / 125 - 130 °C
View Scheme
参考文献
Cope; Fenton
Journal of the American Chemical Society, 1951 , vol. 73, p. 1668,1672
反应条件
1: CCl4; N-bromo-succinimide
2: acetic acid
3: ethanolic NaOH
4: chromium (VI)-oxide; acetic acid
View Scheme
参考文献
Cope; Fenton
Journal of the American Chemical Society, 1951 , vol. 73, p. 1668,1672
反应条件
1: 95 percent / NBS / CCl4 / Heating
2: 79 percent / t-BuOK / tetrahydrofuran / 0 - 20 °C
3: 0.87 g / Br2 / CCl4
4: 87 percent / t-BuOK / tetrahydrofuran / 0 °C
View Scheme
参考文献
Chaffins, Sterling; Brettreich, Michael; Wudl, Fred
Synthesis, 2002 , # 9 p. 1191 - 1194
