1,3,5-三叔丁基苯合成路线 (共 102 条)
反应条件
copper dichloride; palladium dichloride in butan-1-ol; benzene T=40°C; 12 h;
参考文献
Journal of Organic Chemistry, , vol. 66, # 10 p. 3627 - 3629
反应条件
aluminium trichloride T=-40 - -10°C; Friedel-Crafts alkylation; 3 h;
参考文献
Angewandte Chemie - International Edition, , vol. 42, # 20 p. 2258 - 2260
反应条件
N,N,N',N'-tetramethyl-7,8-dihydro-6H-dipyrido[1,2-a;2',1'-c][1,4] diazepine-2,12-diamine in N,N-dimethyl-formamide T=20°C; Inert atmosphere;
参考文献
Organic Letters, , vol. 10, # 6 p. 1227 - 1230
反应条件
η5-cyclopentadienyl dicarbonyl cobalt in water T=380°C; P=187515 Torr; 2 h; cyclotrimerization of acetylenes; Product distributionMechanism;
参考文献
Journal of Organometallic Chemistry, , vol. 570, # 1 p. 121 - 127
反应条件
1: With potassium hydride in tetrahydrofuran T=20°C; 2: in benzene-d6 T=60°C; 1 h;
参考文献
Heterocycles, , vol. 76, # 2 p. 981 - 987
反应条件
1: 2,4,6-tri-tertbutylbromobenzene With magnesium in tetrahydrofuran Heating; 2: 2,4,6-tribromo-1-iodobenzene With magnesium in tetrahydrofuran 4 h; Heating; 3: With hydrogenchloride cooling;
参考文献
Journal of the American Chemical Society, , vol. 126, # 19 p. 6150 - 6163
反应条件
lt;Ti(OC6H3Ph2-2,6)2(C12H20)gt;
参考文献
Journal of the American Chemical Society, , vol. 119, # 33 p. 7685 - 7693
反应条件
1: With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 1 h; Inert atmosphere; 2: With trichlorophosphate in tetrahydrofuran; hexane T=-78 - 20°C;
参考文献
Dalton Transactions, , vol. 42, # 5 p. 1437 - 1450
反应条件
sodium T=200°C; Stickstoff;
参考文献
Journal of the American Chemical Society, , vol. 76, p. 2349,2351
反应条件
aluminium trichloride T=-3°C;
参考文献
Journal of the American Chemical Society, , vol. 76, p. 2349,2351
Canadian Journal of Chemistry, , vol. 33, p. 672,675
Journal of the American Chemical Society, , vol. 77, p. 5735