in diethyl ether to suspn. of Fe complex in ether Me3PCH2 dissolved in ether added dropwise at room temp., allowed to react for 45 h; filtered, concd. in vac., treated with pentane, ppt. washed with pentane, dried in vac.; elem. anal.;
参考文献
Journal of Organometallic Chemistry, , vol. 235, # 1 p. C1 - C6
→
反应条件
in not given
参考文献
Chemische Berichte, , vol. 105, p. 3382 - 3388
Ag: MVol.B7, 1.23.2.1, page 199 - 202
→
反应条件
in benzene Cr complex dissolved in benzene, treated with Me3P=CH2, stirred at roomtemp. for 30 min;
参考文献
Blau, Herbert; Griessmann, Karl-Heinz; Malisch, Wolfgang
Journal of Organometallic Chemistry, 1984 , vol. 264, # 3 p. C1 - C4