5-甲基苯并-2,1,3-噻唑合成路线 （共 13 条）
反应条件
anhydrous sulfurous acid T=180°C;
参考文献
Chemische Berichte, , vol. 22, p. 2897
反应条件
N4S4 in toluene 24 h; Heating;
参考文献
Mataka, Shuntaro; Takahashi, Kazufumi; Shiwaku, Sohgo; Tashiro, Masashi
Journal of Chemical Research, Miniprint, 1985 , # 11 p. 3649 - 3665
参考文献
Zhurnal Obshchei Khimii, , vol. 27, p. 1570,1572; engl. Ausg. S. 1643, 1645
反应条件
methanol; samarium diiodide in tetrahydrofuran T=20°C; 0.333333 h;
参考文献
Fan, Xuesen; Zhang, Xinying; Zhang, Yongmin
Journal of Chemical Research, 2005 , # 1 p. 21 - 22
反应条件
hydrogen bromide; bromine in water T=125°C; 6 h;
参考文献
Peng, Qiang; Lim, Siew-Lay; Wong, Ivy Hoi-Ka; Xu, Jun; Chen, Zhi-Kuan
Chemistry - A European Journal, 2012 , vol. 18, # 38 p. 12140 - 12151
反应条件
1: 4.8 g / NBS; AIBN / CHCl3 / 16 h / Heating 2: 2.66 g / CaCO3; water / dioxane / 3 h / Heating View Scheme
参考文献
Pesin,V.G. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1964 , vol. 34, p. 1272 - 1276,1270 - 1273
参考文献
Pesin,V.G. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1964 , vol. 34, p. 1272 - 1276,1270 - 1273
反应条件
N-bromosuccinmide in chloroform
参考文献
Abbott Laboratories
Patent: US6593335 B1, 2003 ;
US 6593335 B1
反应条件
1: 4.8 g / NBS; AIBN / CHCl3 / 16 h / Heating 2: 2.66 g / CaCO3; water / dioxane / 3 h / Heating 3: 1.9 g / MnO2 / CHCl3 / 20 °C View Scheme
参考文献
Sekikawa
Bulletin of the Chemical Society of Japan, 1959 , vol. 32, p. 551
反应条件
sodium nitrate; sulfuric acid T=95 - 100°C;
参考文献
Pesin,V.G.; Sergeev,V.A.
Chemistry of Heterocyclic Compounds (New York, NY, United States), 1967 , vol. 3, p. 662 - 666
Khimiya Geterotsiklicheskikh Soedinenii, 1967 , vol. 3, # 5 p. 839 - 844
