5-甲硫基-1-苯基-1H-四氮唑合成路线 （共 15 条）
反应条件
sodium hydroxide; tetrabutylammomium bromide in chloroform T=20°C; Methylation; 3 h;
参考文献
Gol'tsberg; Koldobskii
Russian Journal of Organic Chemistry, 1996 , vol. 32, # 8 p. 1194 - 1201
反应条件
1: phenyl isothiocyanate With pyridine; sodium azide in water T=20°C; 2 h; 2: methyl iodide in tetrahydrofuran; water T=20°C; 6 h; regioselective reaction;
参考文献
Han, Sam Yong; Lee, Je Woo; Kim, Hee-Jung; Kim, Yong-Joo; Lee, Soon W.; Gyoung, Young Soo
Bulletin of the Korean Chemical Society, 2012 , vol. 33, # 1 p. 55 - 59
反应条件
tetrabutylammomium bromide; potassium carbonate T=90°C; P=760.051 Torr; 5 h;
参考文献
Xie, Jian-Gang; Quan, Jing; Li, Shu-Bai; Zheng, Yan; Zhu, Li-Min
Synthetic Communications, 2011 , vol. 41, # 6 p. 871 - 878
反应条件
sodium hydroxide T=20°C; Methylation; 2 h;
参考文献
Gol'tsberg; Koldobskii
Russian Journal of Organic Chemistry, 1996 , vol. 32, # 8 p. 1194 - 1201
反应条件
1-n-butyl-3-methylimidazolium chloride T=110°C; 1.5 h; regioselective reaction;
参考文献
Xie, Jiangang; Wu, Chengyao; Christopher, Branford White; Quan, Jing; Zhu, Limin
Phosphorus, Sulfur and Silicon and the Related Elements, 2011 , vol. 186, # 1 p. 31 - 37
反应条件
diethyl ether T=100°C;
参考文献
Chemische Berichte, , vol. 28, p. 80
反应条件
in chloroform T=20°C; Methylation;
参考文献
Russian Journal of Organic Chemistry, , vol. 32, # 8 p. 1194 - 1201
反应条件
in chloroform T=20°C; Methylation;
参考文献
Russian Journal of Organic Chemistry, , vol. 32, # 8 p. 1194 - 1201
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2>124, p. 275
参考文献
Ber. Dtsch. Chem. Ges., , vol. 28, p. 74 - 81
Ag: MVol.B7, 1.20.2.6.4, page 57 - 58
