1,1,4,4-甲苯基-1,3-丁二烯合成路线 （共 91 条）
反应条件
[bmim(HSO3C4)][HSO4]; aluminium in carbon dioxide T=45°C; Ullmann reaction; P=116262 Torr; 12 h; Supercritical conditions;
参考文献
Cheng, Jinsheng; Tang, Longhua; Xu, Jingying
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 18 p. 3275 - 3286
反应条件
lithium aluminium tetrahydride; titanium(III) chloride in tetrahydrofuran 3 h; Heating;
参考文献
Walborsky, H. M.; Wuest, H. H.
Journal of the American Chemical Society, 1982 , vol. 104, # 21 p. 5807 - 5808
反应条件
copper(l) iodide; cesium fluoride in acetonitrile T=20°C; 3 h;
参考文献
Itami, Kenichiro; Ushiogi, Yousuke; Nokami, Toshiki; Ohashi, Youichi; Yoshida, Jun-Ichi
Organic Letters, 2004 , vol. 6, # 21 p. 3695 - 3698
反应条件
1: With Hg(II) trifluoroacetate in benzene T=0°C; Substitution; 0.25 h; 2: With triethylamine; palladium dichloride in benzene T=0°C; Coupling reaction; 0.25 h;
参考文献
Feit, Ben-Ami; Buzhansky, Ludmila
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 11 p. 1777 - 1782
反应条件
ZnCl2*Et2O; anhydrous phosphine T=-196 - 90°C; P=9000.9 - 97509.8 Torr; 37 h; Inert atmosphereAutoclave;
参考文献
Pichota, Arkadius; Gramlich, Volker; Bichsel, Hans-Ulrich; Styner, Thomas; Knoepfel, Thomas; Wuensch, Ralf; Hintermann, Tobias; Schweizer, W. Bernd; Beck, Albert K.; Seebach, Dieter
Helvetica Chimica Acta, 2012 , vol. 95, # 8 p. 1273 - 1302
反应条件
NiCl2((PPh3)P)2 in toluene Heating;
参考文献
Journal of the American Chemical Society, , vol. 111, # 25 p. 9119 - 9121
反应条件
Lawesson's reagent in toluene 0.5 h; Heating;
参考文献
Nishio, Takehiko
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1993 , # 10 p. 1113 - 1118
反应条件
NiBr2(PPh3)2; triphenylphosphine; zinc in N,N-dimethyl-formamide T=20°C; 8 h;
参考文献
Sasaki, Ken; Nakao, Kikuji; Kobayashi, Yoshihiko; Sakai, Mutsuji; Uchino, Norito; et al.
Bulletin of the Chemical Society of Japan, 1993 , vol. 66, # 8 p. 2446 - 2448
反应条件
1: 99 percent / P(t-Bu)3; Et3N / Pd2(dba)3*CHCl3 / dioxane / 80 °C 2: 58 percent / CuI; CsF / acetonitrile / 3 h / 20 °C View Scheme
参考文献
Organic Letters, , vol. 6, # 21 p. 3695 - 3698
反应条件
lithium aluminium tetrahydride; titanium(III) chloride in tetrahydrofuran 3 h; Heating;
参考文献
Journal of the American Chemical Society, , vol. 104, # 21 p. 5807 - 5808
