2-氧代吡咯烷-1-羧酸苄酯合成路线 （共 14 条）
反应条件
1: pyrrolidin-2-one With n-butyllithium in tetrahydrofuran 2: benzyl chloroformate in tetrahydrofuran
参考文献
Peroche, Sandrine; Remuson, Roland; Gelas-Mialhe, Yvonne; Gramain, Jean-Claude
Tetrahedron Letters, 2001 , vol. 42, # 28 p. 4617 - 4619
反应条件
sodium periodate; RuCl3 monohydrate in tetrachloromethane; water; acetonitrile T=20°C; 16 h;
参考文献
Huang, Wei; Ma, Jing-Yi; Yuan, Mu; Xu, Long-Fei; Wei, Bang-Guo
Tetrahedron, 2011 , vol. 67, # 40 p. 7829 - 7837
反应条件
oxalyl dichloride in dichloromethane T=20°C; 4 h;
参考文献
Guenin, Erwann; Monteil, Maelle; Bouchemal, Nadia; Prange, Thierry; Lecouvey, Marc
European Journal of Organic Chemistry, 2007 , # 20 p. 3380 - 3391
参考文献
Karl Thomae GmbH
Patent: US5681841 A1, 1997 ;
反应条件
4-(N,N-dimethlyamino)pyridine; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride
参考文献
Gibbs, Gary; Hateley, Martin J.; McLaren, Lee; Welham, Matthew; Willis, Christine L.
Tetrahedron Letters, 1999 , vol. 40, # 5 p. 1069 - 1072
反应条件
lithium hexamethyldisilazane 1>) THF, hexane, -78 deg C, 30 min, 2.) THF, hexane, a) -78 deg C, 30 min, b) RT, 1.5 h; Yield given. Multistep reaction;
参考文献
Louwrier, Saskia; Tuynman, Antonin; Hiemstra, Henk
Tetrahedron, 1996 , vol. 52, # 7 p. 2629 - 2646
反应条件
polymer-supported diphenylphosphoryl azide; triethylamine 24 h; Heating;
参考文献
Lu, Yuhua; Taylor, Richard T.
Heterocycles, 2004 , vol. 62, p. 869 - 876
反应条件
hydrogen; palladium on activated charcoal in methanol 24 h;
参考文献
Guenin, Erwann; Monteil, Maelle; Bouchemal, Nadia; Prange, Thierry; Lecouvey, Marc
European Journal of Organic Chemistry, 2007 , # 20 p. 3380 - 3391
反应条件
magnesium 1.) THF, 2.) -78 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Giovannini, Arianna; Savoia, Diego; Umani-Ronchi, Achille
Journal of Organic Chemistry, 1989 , vol. 54, # 1 p. 228 - 234
反应条件
Cp*RuCl{(C6H5)2P-(CH2)2NH2-κ2-P,N}; potassium tert-butylate; hydrogen in tert-butyl alcohol T=80°C; P=22502.3 Torr; 24 h; Autoclave;
参考文献
Ito, Masato; Koo, Lee Wei; Himizu, Akio; Kobayashi, Chika; Sakaguchi, Ayaka; Ikariya, Takao
Angewandte Chemie - International Edition, 2009 , vol. 48, # 7 p. 1324 - 1327
