反应条件
1: oxalyl dichloride / toluene / 4 h / |Reflux; |Inert atmosphere
2: triethylamine / dichloromethane / 72 h / |Reflux; |Inert atmosphere
3: RuCl2(tricyclohexylphosphine)2(benzylidene) / dichloromethane / 16 h / 40 °C / |Inert atmosphere
4: palladium on activated charcoal; hydrogen / ethanol / 2 h / 20 °C / |Inert atmosphere
View Scheme
参考文献
Ouadi, Ali; Habold, Caroline; Keller, Murielle; Bekaert, Virgile; Brasse, David
RSC Advances, 2013 , vol. 3, # 41 p. 19040 - 19050