2-(2’-硝基苯偶氮)-4-甲基酚合成路线 （共 28 条）
反应条件
1: 2-nitro-aniline With hydrogenchloride; sodium nitrite in water T=0°C; 0.5 h; 2: p-cresol With sodium hydroxide in water; isopropyl alcohol T=20°C; Cooling; 3: With hydrogenchloride in water; isopropyl alcohol T=20°C;
参考文献
Farkas, Renata; Toerincsi, Mercedesz; Kolonits, Pal; Fekete, Jenoe; Alonso, Oscar Jimenez; Novak, Lajos
Central European Journal of Chemistry, 2010 , vol. 8, # 2 p. 300 - 307
参考文献
Goldschmidt; Brubacher
Chemische Berichte, 1891 , vol. 24, p. 2313
反应条件
carbon monoxide; triethylamine in 1,2-dichloro-benzene T=200°C; P=60800 Torr; 8 h; Further byproducts given;
参考文献
Gazzetta Chimica Italiana, , vol. 123, # 12 p. 683 - 686
反应条件
carbon monoxide; triethylamine in 1,2-dichloro-benzene T=200°C; P=53200 Torr; 5 h; other tertiary amines, var. solvent, var. time; Product distribution;
参考文献
Pizzotti, Maddalena; Ragaini, Fabio; Cenini, Sergio
Gazzetta Chimica Italiana, 1993 , vol. 123, # 12 p. 683 - 686
反应条件
hydrogen; nickel in water; isopropyl alcohol T=59.85°C; Title compound not separated from byproducts;
参考文献
Lefedova
Russian Journal of Physical Chemistry A, 2003 , vol. 77, # 8 p. 1266 - 1269
反应条件
hydrogen; nickel in water; isopropyl alcohol T=1.85°C; P=760 Torr; Product distributionKinetics;
参考文献
Zuenko; Nemtseva; Lefedova; Nikolaev
Russian Journal of Physical Chemistry A, 2004 , vol. 78, # 6 p. 877 - 881
反应条件
2-Bromo-2-nitropropane; zinc in methanol; dichloromethane 21 h; Ambient temperature;
参考文献
Kim, Byeong Hyo; Lee, Yoon Seok; Kwon, Woong; Jin, Youngoo; Tak, Jung Ae; Jun, Young Moo; Baik, Woonphil; Lee, Byung Min
Heterocycles, 1998 , vol. 48, # 12 p. 2581 - 2592
反应条件
hydrogen; nickel in water; isopropyl alcohol T=59.85°C; Title compound not separated from byproducts;
参考文献
Lefedova
Russian Journal of Physical Chemistry A, 2003 , vol. 77, # 8 p. 1266 - 1269
反应条件
hydrogen; nickel in water; isopropyl alcohol T=1.85°C; P=760 Torr; Product distributionKinetics;
参考文献
Zuenko; Nemtseva; Lefedova; Nikolaev
Russian Journal of Physical Chemistry A, 2004 , vol. 78, # 6 p. 877 - 881
反应条件
2-Bromo-2-nitropropane; zinc in methanol; dichloromethane 21 h; Ambient temperature;
参考文献
Kim, Byeong Hyo; Lee, Yoon Seok; Kwon, Woong; Jin, Youngoo; Tak, Jung Ae; Jun, Young Moo; Baik, Woonphil; Lee, Byung Min
Heterocycles, 1998 , vol. 48, # 12 p. 2581 - 2592
