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乙二醇
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63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
14310-22-6
合成路线
（共 29 条）
1073-67-2
4-氯苯乙烯
+
108-86-1
溴代苯
→
反应条件
14310-22-6
反应条件
1: With sodium acetate in N,N-dimethyl acetamide T=100°C; Heck reaction; Inert atmosphere; 2: With hydrogen in N,N-dimethyl acetamide T=20°C; P=760.051 Torr;
参考文献
Kantam, M. Lakshmi; Chakravarti, Rajashree; Chintareddy, Venkat Reddy; Sreedhar; Bhargava, Suresh
Advanced Synthesis and Catalysis, 2008 , vol. 350, # 16 p. 2544 - 2550
6529-53-9
4-氯苯乙基溴化物
+
100-59-4
苯基氯化镁
→
反应条件
14310-22-6
反应条件
N,N,N',N,-tetramethylethylenediamine; ((Me)N2N)Ni-Cl in tetrahydrofuran T=20°C; Kumada-Corriu-Tamao coupling reaction; 2 h; Inert atmosphere;
参考文献
Vechorkin, Oleg; Proust, Valerie; Hu, Xile
Journal of the American Chemical Society, 2009 , vol. 131, # 28 p. 9756 - 9766
292638-84-7
+
106-39-8
4-溴氯苯
→
反应条件
14310-22-6
反应条件
1: With 5 Pd(II)/C(eggshell); sodium acetate in 1-methyl-pyrrolidin-2-one T=140°C; Heck reaction; 24 h; 2: With 5 Pd(II)/C(eggshell); hydrogen in 1-methyl-pyrrolidin-2-one T=20°C; P=750.075 Torr; 24 h;
参考文献
Cusati, Giuseppe; Wedig, Anja; Djakovitch, Laurent
Letters in Organic Chemistry, 2009 , vol. 6, # 1 p. 77 - 81
5172-02-1
1-氯-4-(苯基乙炔基)苯
→
反应条件
1657-50-7
+
14310-22-6
反应条件
C41H38BFeN3P2; hydrogen in tetrahydrofuran T=20 - 90°C; P=7500.75 Torr; 23 h; Inert atmosphere;
参考文献
Srimani, Dipankar; Diskin-Posner, Yael; Ben-David, Yehoshoa; Milstein, David
Angewandte Chemie - International Edition, 2013 , vol. 52, # 52 p. 14131 - 14134
Angew. Chem., 2013 , vol. 125, # 52 p. 14381 - 14383
1041479-70-2
+
89523-62-6
→
反应条件
2050-68-2
+
14310-22-6
反应条件
(MeCN)2PdCl2; 2-chloro-1,2-diphenyl-ethanone; bis[2-(diphenylphosphino)phenyl] ether in tetrahydrofuran T=60°C; 5 h; chemoselective reaction;
参考文献
Jin, Liqun; Zhao, Yingsheng; Zhu, Lizheng; Zhang, Heng; Lei, Aiwen
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 4 p. 630 - 634
34420-17-2
+
29540-84-9
→
反应条件
14310-22-6
反应条件
potassium carbonate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct in tetrahydrofuran; water Suzuki coupling reaction; 18 h; Heating;
参考文献
Molander, Gary A.; Yun, Chang-Soo
Tetrahedron, 2002 , vol. 58, # 8 p. 1465 - 1470
50793-42-5
→
反应条件
14310-22-6
反应条件
sodium tetrahydroborate; nickel dichloride in methanol T=20°C; 0.166667 h;
参考文献
Khurana, Jitender M.; Kandpal, Bhaskar M.; Kukreja, Gagan; Sharma, Purnima
Canadian Journal of Chemistry, 2006 , vol. 84, # 8 p. 1019 - 1023
1589-82-8
+
873-76-7
→
反应条件
14310-22-6
反应条件
1: 4-chloro-1-hydroxymethyl-benzene With n-butyllithium; chloro-diphenylphosphine 2: With methyl iodide in tetrahydrofuran T=20°C; 1 h; 3: benzyl-magnesium bromide in tetrahydrofuran T=20°C; 1 h;
参考文献
Shintou, Taichi; Kikuchi, Wataru; Mukaiyama, Teruaki
Chemistry Letters, 2003 , vol. 32, # 8 p. 676 - 677
106-43-4
+
108-88-3
→
反应条件
14310-22-6
反应条件
di-tert-butyl peroxide T=140°C; 48 h;
参考文献
Pryor, William A.; Tang, Felicia Y.; Tang, Robert H.; Church, Daniel F.
Journal of the American Chemical Society, 1982 , vol. 104, # 10 p. 2885 - 2891
1041479-62-2
→
反应条件
14310-22-6
反应条件
dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct; 2-chloro-1,2-diphenyl-ethanone in tetrahydrofuran T=60°C; 5 h; chemoselective reaction;
参考文献
Jin, Liqun; Zhao, Yingsheng; Zhu, Lizheng; Zhang, Heng; Lei, Aiwen
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 4 p. 630 - 634
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