N-(3,4-二甲氧基苯乙基)甲酰胺合成路线 （共 25 条）
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 22, # 7 p. 2585 - 2589
反应条件
in tetrahydrofuran T=20°C; 16 h;
参考文献
Organic Letters, , vol. 12, # 7 p. 1396 - 1399
反应条件
acetic anhydride 1.) 60 deg C, 30 min, 2.) 20 deg C, overnight;
参考文献
Tetrahedron, , vol. 54, # 26 p. 7485 - 7496
反应条件
n-butyllithium in tetrahydrofuran T=0°C; 16 h;
参考文献
Tetrahedron Letters, , vol. 29, # 31 p. 3865 - 3868
反应条件
in methanol 12 h; Ambient temperature;
参考文献
Tetrahedron, , vol. 39, # 6 p. 905 - 912
参考文献
Journal of Scientific and Industrial Research, , vol. 17B, p. 219,223
反应条件
1: LiAlH4; diethyl ether 2: chloral View Scheme
参考文献
Journal of Scientific and Industrial Research, , vol. 17B, p. 219,223
反应条件
PPA in dichloromethane T=50°C; 2 h;
参考文献
Ivanov, Iliyan; Nikolova, Stoyanka; Statkova-Abeghe, Stela; Angelov, Plamen
Heterocycles, 2006 , vol. 68, # 2 p. 387 - 393
反应条件
1.1: 14.48 g / phosphoryl chloride / toluene / 1 h / Heating 2.1: 59.7 percent / bromophenol blue; conc. hydrochloric acid / methanol / 0 - 20 °C 3.1: KHMDS / tetrahydrofuran / 3 h / -78 °C 3.2: 177.5 mg / aq. NiCl2 / methanol / 20 °C View Scheme
参考文献
Ivanov, Iliyan; Nikolova, Stoyanka; Statkova-Abeghe, Stela; Angelov, Plamen
Heterocycles, 2006 , vol. 68, # 2 p. 387 - 393
反应条件
1.1: 14.48 g / phosphoryl chloride / toluene / 1 h / Heating 2.1: 59.7 percent / bromophenol blue; conc. hydrochloric acid / methanol / 0 - 20 °C 3.1: KHMDS / tetrahydrofuran / 3 h / -78 °C 3.2: 557.6 mg / aq. NiCl2 / methanol / 20 °C 4.1: triethylamine; formic acid / (R,R)-Noyori's catalyst / dimethylformamide / 4.5 h / 20 °C View Scheme
参考文献
Werner, Frank; Blank, Nancy; Opatz, Till
European Journal of Organic Chemistry, 2007 , # 23 p. 3911 - 3915
