Tris-SO4 buffer in water; dimethyl sulfoxide
T=22°C; pH=7.5; 5 h; Title compound not separated from byproducts.;
参考文献
Elenkov, Maja Majerie; Hoeffken, H. Wolfgang; Tang, Lixia; Hauer, Bernhard; Janssen, Dick B.
Advanced Synthesis and Catalysis, 2007 , vol. 349, # 14-15 p. 2279 - 2285
1: sodium cyanide With ammonia in water
T=25°C; P=1125.11 Torr; 0.5 h;
2: phenylacetaldehyde With acetic acid in water
T=35°C; 4.75 h;
3: With hydrogenchloride in 1,4-dioxane; diethyl ether
参考文献
DSM IP Assets B.V.
Patent: EP1352894 A1, 2003 ;
Location in patent: Page/Page column 4 ;
