反应条件
Na/Hg in tetrahydrofuran Ar, Schlenk; Re-compd. addn. to 2 parts of stirred THF-Na/Hg (1percent Na) mixt., two parts combining, org. compd. addn. dropwise at 0°C, solvent removal after 2-4 h (reduced pressure), residue extn. (hexane), 4 extracts combination, hexane removal; column chromy. (silica gel, 2-5percentTHF/hexane), recrystn. (hexane, 10°C); elem. anal.;
参考文献
Alexander, John J.; Padolik, Laura L.; Ho, Douglas M.
Inorganica Chimica Acta, 1995 , vol. 240, p. 495 - 502