二氯(N,N,N’,N’-四甲基乙二胺)钯合成路线 （共 9 条）
反应条件
in acetone refluxing (3 h), stirring overnight; filtration, washing (acetone, Et2O);
参考文献
Vicente, Jose; Abad, Jose Antonio; Chicote, Maria-Teresa; Abrisqueta, Maria-Dolores; Lorca, Jose-Angel; Ramirez De Arellano, M. Carmen
Organometallics, 1998 , vol. 17, # 8 p. 1564 - 1568
反应条件
in acetonitrile treatment of palladium compd. with amine deriv. in acetonitrile at room temp.; recrystn.;
参考文献
Biscoe, Mark R.; Fors, Brett P.; Buchwald, Stephen L.
Journal of the American Chemical Society, 2008 , vol. 130, # 21 p. 6686 - 6687
反应条件
in acetonitrile T=20°C; 1.5 h; Inert atmosphere;
参考文献
Zhao, Qing; Li, Chengxi; Senanayake, Chris H.; Tang, Wenjun
Chemistry - A European Journal, 2013 , vol. 19, # 7 p. 2261 - 2265
反应条件
in acetonitrile refluxing PdCl2-acetonitrile solution; cooling to 20°C; adding tmeda; analysis;
参考文献
Graaf, Wim de; Boersma, Jaap; Smeets, Wilberth J. J.; Spek, Anthony L.; Koten, Gerard van
Organometallics, 1989 , vol. 8, p. 2907 - 2917
反应条件
in dimethyl sulfoxide 100°C, 30 min; monitored by (1)H NMR;
参考文献
Jung, Miso; Suzaki, Yuji; Saito, Takashi; Shimada, Kyoichi; Osakada, Kohtaro
Polyhedron, 2012 , vol. 40, # 1 p. 168 - 174
反应条件
in water Kinetics; React. at 25°C and pH 4-5.;
参考文献
Inorganic Chemistry, , vol. 31, p. 1090 - 1095
反应条件
in water equimolar amounts of reactants; pH adjusted to 3 with 1 M HCl; stirred (80°C, 2 h); crystd. (water, room temp.); recrystd. (water, cooling); elem. anal.;
参考文献
Polyhedron, , vol. 19, # 8 p. 959 - 963
反应条件
in water Kinetics; byproducts: H2O; 16.0-38.7°C, pH=3.8; not isolated; UV spectroscopic monitoring;
参考文献
Inorganica Chimica Acta, , vol. 188, p. 25 - 32
反应条件
perchloric acid Kinetics; byproducts: H2O; excess of Cl(1-), at 25°C, pH adjusted with HClO4 to 4-5;
参考文献
Inorganica Chimica Acta, , vol. 198 - 200, p. 187 - 192
