triethylamine in tetrahydrofuran byproducts: [Et3NH][(H2P)P(O)O], [Et3NH][(H2P)2P(O)]; N2 atm.; dark; molar ratio P2H4: oxidant 1:2, cooling (-78 to -30°C; 4 h 45 min), stirring (25 h, -30°C); followed by NMR;
参考文献
Zeitschrift fuer Anorganische und Allgemeine Chemie, , vol. 621, p. 1689 - 1692
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反应条件
in water under neutral conditions; not isolated, detected by NMR;
hydrogenchloride in water P:V:W = 1:3:9; various pH values;; various product mixture; not isolated; detn. by (31)P- and (51)V-NMR;;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 36, p. 427 - 431
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , p. 473 - 478
