1,4-双(二苯基氨基)苯合成路线 (共 17 条)
反应条件
potassium carbonate; copper in nitrobenzene Phenylation; Ullmann reaction; 8 h; Heating;
参考文献
Getautis; Stanisauskaite; Paliulis; Uss
Journal fuer Praktische Chemie - Practical Applications and Applied Chemistry (Germany), 2000 , vol. 342, # 1 p. 58 - 62
反应条件
1: 87 percent / Pd(dba)2, P(t-Bu)3, t-BuONa / toluene / 1 h / Ambient temperature 2: 85 percent / Pd(dba)2, P(t-Bu)3, t-BuONa / toluene / 1 h / Ambient temperature View Scheme
参考文献
Hartwig, John F.; Kawatsura, Motoi; Hauck, Sheila I.; Shaughnessy, Kevin H.; Alcazar-Roman, Luis M.
Journal of Organic Chemistry, 1999 , vol. 64, # 15 p. 5575 - 5580
反应条件
1: 87 percent / Pd(dba)2, P(t-Bu)3, t-BuONa / toluene / 1 h / Ambient temperature 2: 85 percent / Pd(dba)2, P(t-Bu)3, t-BuONa / toluene / 1 h / Ambient temperature View Scheme
参考文献
Hartwig, John F.; Kawatsura, Motoi; Hauck, Sheila I.; Shaughnessy, Kevin H.; Alcazar-Roman, Luis M.
Journal of Organic Chemistry, 1999 , vol. 64, # 15 p. 5575 - 5580
反应条件
1: 75 percent / Pd(dba)2, P(t-Bu)3, t-BuONa / toluene / 25 h / Ambient temperature 2: 85 percent / Pd(dba)2, P(t-Bu)3, t-BuONa / toluene / 1 h / Ambient temperature View Scheme
参考文献
Hartwig, John F.; Kawatsura, Motoi; Hauck, Sheila I.; Shaughnessy, Kevin H.; Alcazar-Roman, Luis M.
Journal of Organic Chemistry, 1999 , vol. 64, # 15 p. 5575 - 5580
反应条件
potassium hydroxide; copper T=160°C; competitive reaction, var. catalysts; Rate constantMechanism;
参考文献
Paine, Anthony James
Journal of the American Chemical Society, 1987 , vol. 109, # 5 p. 1496 - 1502
反应条件
potassium hydroxide; copper T=160°C; competitive reaction, var. catalysts; Rate constantMechanism;
参考文献
Paine, Anthony James
Journal of the American Chemical Society, 1987 , vol. 109, # 5 p. 1496 - 1502
参考文献
Haeussermann; Bauer
Chemische Berichte, 1899 , vol. 32, p. 1912