(E)-3,7-二甲基-2,6-辛二烯醛合成路线 （共 128 条）
反应条件
nickel sulphate; ammonium hydroxide; sodium hydroxide; dipotassium peroxodisulfate in water
6 h; Ambient temperature;
参考文献
Yamazaki, Shigakazu; Yamazaki, Yasuyuki
Chemistry Letters, 1990 , # 4 p. 571 - 574
反应条件
periodic acid in 1,4-dioxane; water
T=0°C; 1 h;
参考文献
Kikuchi; Mori; Yokoi; et al.
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 1 p. 106 - 113
反应条件
1: 85 percent / NaH / tetrahydrofuran / 0 deg C, then Rt 1 h
2: 1.) Dibal; 2.) silica gel / 1.) petroleum ether, hexane, -60 deg C, then 10 deg C over 1.5 h; 2.) petroleum ether, hexane, water, -30 deg C, then 0 deg C, 1 h
View Scheme
参考文献
Gebhard, R.; Courtin, J. M. L.; Shadid, J. B.; Haveren, J. van; Haeringen, C. J. van; Lugtenburg, J.
Recueil des Travaux Chimiques des Pays-Bas, 1989 , vol. 108, # 6 p. 207 - 214
反应条件
dihydrogen peroxide; sodium acetate in water
T=27°C; pH=5; 1 h; Enzymatic reaction;
参考文献
Zelena, Kateryna; Hardebusch, Bjoern; Huelsdau, Baerbel; Berger, Ralf G.; Zorn, Holger
Journal of Agricultural and Food Chemistry, 2009 , vol. 57, # 21 p. 9951 - 9955
反应条件
tris(triphenylphosphine)ruthenium(II) chloride; sodium carbonate; benzaldehyde in 1,2-dichloro-ethane
T=90°C; 4 h; Schlenk techniqueInert atmosphere; Reagent/catalystTemperature;
参考文献
Ren, Kai; Hu, Bei; Zhao, Mengmeng; Tu, Yahui; Xie, Xiaomin; Zhang, Zhaoguo
Journal of Organic Chemistry, 2014 , vol. 79, # 5 p. 2170 - 2177
反应条件
tert.-butylhydroperoxide; Gel-bis(phosphonomethyl)amino polymer Vanadium(V) in water; benzene
T=80°C; 4 h; Yield given;
参考文献
Yokoyama, Toshiro; Nishizawa, Masato; Kimura, Tetsuo; Suzuki, Toshishige M.
Chemistry Letters, 1983 , p. 1703 - 1706
反应条件
alpha-methylbenzyl hydroperoxide; Na12Mn2Zn3W19O70H4 in 1,2-dichloro-ethane
T=50°C; 24 h; Title compound not separated from byproducts;
参考文献
Adam, Waldemar; Alsters, Paul L.; Neumann, Ronny; Saha-Moeller, Chantu R.; Seebach, Dieter; Beck, Albert K.; Zhang, Rui
Journal of Organic Chemistry, 2003 , vol. 68, # 21 p. 8222 - 8231
反应条件
2,2,6,6-tetramethyl-1-piperidinyloxy, free radical in tert-butyl alcohol
T=25°C; pH=11.5; aq. sodium carbonate/bicarbonate bufferElectrolysis; optical yield given as percent de;
参考文献
Hill-Cousins, Joseph T.; Kuleshova, Jekaterina; Green, Robert A.; Birkin, Peter R.; Pletcher, Derek; Underwood, Toby J.; Leach, Stuart G.; Brown, Richard C. D.
ChemSusChem, 2012 , vol. 5, # 2 p. 326 - 331
反应条件
dihydrogen peroxide; molecular sieve in acetone
8 h; Heating; Yield given;
参考文献
Kumar, Rajiv; Pais, Godwin C. G.; Pandey, Bipin; Kumar, Pradeep
Journal of the Chemical Society, Chemical Communications, 1995 , # 13 p. 1315 - 1316
反应条件
iodosylbenzene; sodium lauryl sulfate; [14C]-Tetramethylammonium bromide; [5,10,15,20-tetrakis(2,6-dichlorophenyl)porphinato]iron(III) chloride in water
T=20°C; Oxidation; pH=4.0; 1 h; Product distribution; Further Variations:ReagentsSolventspH-values;
参考文献
Chauhan; Parkash, Som; Mohapatra
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, 1997 , vol. 36, # 4 p. 312 - 317
