1: N-methylaniline With n-butyllithium in tetrahydrofuran T=-70°C; Inert atmosphere; 2: With carbon dioxide in tetrahydrofuran T=0 - 10°C; Inert atmosphere; 3: chloro-diphenylphosphine Further stages;
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Lightburn, Thomas E.; Dombrowski, Michael T.; Tan, Kian L.
Journal of the American Chemical Society, 2008 , vol. 130, # 29 p. 9210 - 9211
1: N-methylaniline With n-butyllithium in hexane T=20°C; Inert atmosphereSchlenk techniqueGlovebox; 2: With carbon dioxide in diethyl ether; hexane T=-78°C; Inert atmosphereSchlenk techniqueGlovebox; 3: PhOPPh2 Further stages;
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Jun, Sung Hae; Park, Ji Hae; Lee, Chun Sun; Park, Seong Yeon; Go, Min Jeong; Lee, Junseong; Lee, Bun Yeoul
Organometallics, 2013 , vol. 32, # 24 p. 7357 - 7365