1-羟基甲基-1-甲基环己烷合成路线 （共 32 条）
反应条件
1: SOCl2; Et3N / CH2Cl2 / 1 h / 0 °C 2: 92 percent / toluene / 1 h / 0 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 41, # 16 p. 2945 - 2948
反应条件
mercury 48 h; HeatingIrradiation; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Journal of the American Chemical Society, , vol. 111, # 8 p. 2946 - 2953
反应条件
1: 80 percent / pyridine 2: LiAlH4 / tetrahydrofuran / 60 °C View Scheme
参考文献
Chemistry Letters, , p. 1785 - 1788
反应条件
1: H2SO4 / 5 - 7 °C 2: LiAlH4 View Scheme
参考文献
Journal of Organic Chemistry, , vol. 30, p. 350 - 354
反应条件
1: formic acid; H2SO4 2: lithium alanate; diethyl ether View Scheme
参考文献
Justus Liebigs Annalen der Chemie, , vol. 618, p. 251,261
反应条件
1: formic acid; H2SO4 2: lithium alanate; diethyl ether View Scheme
参考文献
Justus Liebigs Annalen der Chemie, , vol. 618, p. 251,261
反应条件
1: formic acid; H2SO4 2: lithium alanate; diethyl ether View Scheme
参考文献
Justus Liebigs Annalen der Chemie, , vol. 618, p. 251,261
反应条件
1: formic acid; H2SO4 2: lithium alanate; diethyl ether View Scheme
参考文献
Justus Liebigs Annalen der Chemie, , vol. 618, p. 251,261
反应条件
1: Raney nickel; ethyl acetate / 180 °C / 73550.8 Torr / Hydrogenation 2: lithium alanate; diethyl ether View Scheme
参考文献
Bulletin de la Societe Chimique de France, , p. 600,606
反应条件
1: 86.9 percent / NaH / dimethylsulfoxide / 0.5 h / 70 °C 2: hydrogen / 10percent Pd-C / methanol / 760 Torr / Ambient temperature 3: 1.) NaNO2, conc. HCl, 2.) Cu2O / 1.) acetone, water, 5 deg C, 30 min, 2.) acetone, water, 35 deg C View Scheme
参考文献
Sohda; Mizuno; Imamiya; Sugiyama; Fujita; Kawamatsu
Chemical and Pharmaceutical Bulletin, 1982 , vol. 30, # 10 p. 3580 - 3600
