3,3ˊ-亚氨基双-1-丙醇合成路线 （共 20 条）
反应条件
1: With water 24 h; Heating / reflux; 2: With potassium hydroxide in water
参考文献
Hong Kong Polytechnic University; Victor Snieckus
Patent: US2006/69249 A1, 2006 ;
Location in patent: Page/Page column 3 ;
反应条件
hydrogen; palladium on activated charcoal in methanol P=2280 Torr; 2 h;
参考文献
Groth, Andrew M.; Lindoy, Leonard F.; Meehan, George V.
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 13 p. 1553 - 1558
反应条件
lithium aluminium tetrahydride in diethyl ether 1.) room temperature, 1 h, 2.) reflux, 24 h;
参考文献
Denney,D.B.; Denney,D.Z.; Hammond,P.J.
Journal of the American Chemical Society, 1980 , vol. 102, p. 5073
反应条件
lithium aluminium tetrahydride in diethyl ether T=25°C; 5 h;
参考文献
Hahn, Ekkehardt F.; Rupprecht, Stefan
Chemische Berichte, 1991 , vol. 124, # 3 p. 481 - 486
反应条件
sodium carbonate in ethanol 24 h; Heating;
参考文献
Journal of the Chemical Society, Dalton Transactions, , # 12 p. 1863 - 1871
反应条件
1: LAH 2: H2 / Pd(OH)2 View Scheme
参考文献
Journal of Organic Chemistry, , vol. 65, # 24 p. 8367 - 8371
反应条件
lithium aluminium tetrahydride in tetrahydrofuran rt 30 min, reflux 2 h; Yield given;
参考文献
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), , p. 1361 - 1364
反应条件
nickel kieselguhr T=60 - 70°C; Hydrogenation.unter Druck;
参考文献
DE573983 , ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 18, p. 818
反应条件
alkali Kochen des Reaktionsprodukts mit Natrium und Isoamylalkohol;
参考文献
Zhurnal Obshchei Khimii, , vol. 8, p. 1547
Chem. Zentralbl., , vol. 110, # I p. 4951
反应条件
T=60 - 70°C; P=36775.4 Torr; Hydrogenation;
参考文献
DE573983 , ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 18, p. 818
