4-[[(1,1-二甲基乙基)二甲基甲硅烷基]氧基]-苯甲醇合成路线 （共 19 条）
反应条件
1.1: 70 percent / methanesulfonyl chloride; Et3N / CH2Cl2 / 1.5 h / 20 °C 2.1: Mg; 1,2-dibromoethane / tetrahydrofuran / 0.5 h / Heating 2.2: 72 percent / tetrahydrofuran / 1 h / -78 °C 3.1: 27 percent / conc. HCl / dioxane / 8 h / Heating View Scheme
参考文献
Adamczyk, Maciej; Johnson, Donald D.; Mattingly, Phillip G.; Pan, You; Reddy, Rajarathnam E.
Organic Preparations and Procedures International, 2001 , vol. 33, # 5 p. 477 - 485
反应条件
1: 85 percent / iodine / CH2Cl2 / 0.5 h 2: 75 percent / iodine / methanol / 2 h / Heating View Scheme
参考文献
Kumar, H. M. Sampath; Reddy, B. V. Subba; Reddy, E. Jagan; Yadav, J. S.
Chemistry Letters, 1999 , # 9 p. 857 - 858
反应条件
2,4,6-trichloro-1,3,5-triazine; dimethyl sulfoxide T=20°C; 0.333333 h; chemoselective reaction;
参考文献
Sun, Lili; Peng, Guisheng; Niu, Hongmei; Wang, Qiang; Li, Chunbao
Synthesis, 2008 , # 24 art. no. F17308SS, p. 3919 - 3924
反应条件
triethylamine in water; N,N-dimethyl-formamide
参考文献
JNC CORPORATION; NATIONAL UNIVERSITY CORPORATION TOKYO MEDICAL AND DENTAL UNIVERSITY
Patent: US2011/244481 A1, 2011 ;
反应条件
sulfated SnO2 in methanol
T=20°C; 0.25 h;
参考文献
Bhure, Mahesh H.; Kumar, Indresh; Natu, Arun D.; Rode, Chandrashekhar V.
Synthetic Communications, 2008 , vol. 38, # 3 p. 346 - 353
反应条件
sodium tetrahydroborate; silica gel in dichloromethane
T=0°C; 0.0833333 h;
参考文献
Quiroz-Florentino, Hector; Hernandez-Benitez, R. Israel; Avina, Judit A.; Burgueno-Tapia, Eleuterio; Tamariz, Joaquin
Synthesis, 2011 , # 7 p. 1106 - 1112
反应条件
sodium borohydride; sodium chloride in tetrahydrofuran; methanol; water; N,N-dimethyl-formamide
参考文献
Takeda Chemical Industries, Ltd.
Patent: US6251926 B1, 2001 ;
反应条件
lithium aluminium tetrahydride in tetrahydrofuran
T=0 - 20°C; 20.1667 h;
参考文献
Plazuk, Damian; Rychlik, Blazej; Blauz, Andrzej; Domagala, Slawomir
Journal of Organometallic Chemistry, 2012 , vol. 715, p. 102 - 112
反应条件
hydrogenchloride in dichloromethane
参考文献
ELI LILLY AND COMPANY
Patent: EP811621 A2, 1997 ;
EP 0811621 A2
反应条件
ethane-1,2-dithiol; nickel dichloride in methanol; dichloromethane
T=20°C; 0.5 h;
参考文献
Khan, Abu T.; Islam, Samimul; Choudhury, Lokman H.; Ghosh, Subrata
Tetrahedron Letters, 2004 , vol. 45, # 52 p. 9617 - 9621
