4-溴-2-(环戊基氧基)苯甲醚合成路线 （共 22 条）
反应条件
triphenylphosphine; diethylazodicarboxylate in toluene T=20°C; 2 h; Inert atmosphere;
参考文献
Woodring, Jennifer L.; Bland, Nicholas D.; Ochiana, Stefan O.; Campbell, Robert K.; Pollastri, Michael P.
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 21 p. 5971 - 5974
反应条件
potassium carbonate in acetone 24 h; Heating;
参考文献
Meyers, A. I.; Snyder, Lawrence
Journal of Organic Chemistry, 1993 , vol. 58, # 1 p. 36 - 42
反应条件
triphenylphosphine in tetrahydrofuran
参考文献
Aventis Pharmaceuticals Products Inc.
Patent: US6306873 B1, 2001 ;
US 6306873 B1
反应条件
potassium carbonate in hexane; acetonitrile
参考文献
American Home Products Corporation
Patent: US5691376 A1, 1997 ;
反应条件
potassium carbonate in hexane; acetonitrile
参考文献
American Home Products Corporation
Patent: US5650444 A1, 1997 ;
反应条件
1: 97 percent / H2SO4 / 6 h / 100 °C 2: 99 percent / NBS / acetonitrile / 10 h / 60 °C 3: 95 percent / NaHCO3 / methanol / 3 h / Heating 4: 89 percent / K2CO3 / dimethylformamide / 12 h / 50 °C View Scheme
参考文献
Conde, Jose J.; Mendelson, Wilford
Tetrahedron Letters, 2000 , vol. 41, # 6 p. 811 - 814
反应条件
in N,N-dimethyl-formamide
参考文献
RHONE-POULENC RORER LIMITED
Patent: EP741707 B1, 1998 ;
反应条件
1.1: 3-chloroperoxybenzoic acid / CH2Cl2 / 72 h / 0 - 20 °C 1.2: 92 percent / 2 M NaOH / diethyl ether 2.1: 99 percent / K2CO3 / dimethylformamide / 10 h / 65 °C View Scheme
参考文献
Hulme, Christopher; Poli, Gregory B.; Huang, Fu-Chih; Souness, John E.; Djuric, Stevan W.
Bioorganic and Medicinal Chemistry Letters, 1998 , vol. 8, # 2 p. 175 - 178
反应条件
1: 99 percent / NBS / acetonitrile / 10 h / 60 °C 2: 95 percent / NaHCO3 / methanol / 3 h / Heating 3: 89 percent / K2CO3 / dimethylformamide / 12 h / 50 °C View Scheme
参考文献
Yahya-Meymandi; Mohammadi Ziarani; Shafiee; Foroumadi
Asian Journal of Chemistry, 2011 , vol. 23, # 9 p. 4008 - 4010
反应条件
1: 95 percent / NaHCO3 / methanol / 3 h / Heating 2: 89 percent / K2CO3 / dimethylformamide / 12 h / 50 °C View Scheme
参考文献
Yahya-Meymandi; Mohammadi Ziarani; Shafiee; Foroumadi
Asian Journal of Chemistry, 2011 , vol. 23, # 9 p. 4008 - 4010
