反应条件
HCl in diethyl ether byproducts: (Me2NH2)Cl; N2-atmosphere; addn. of slight excess catechol to B-compd., stirring at room temp. for several h; cooling in ice/water, dropwise addn. of excess 1 M HCl in Et2O, stirringat room temp. for 10 h, solvent removal (vac.), extn. into PhMe, filtra tion (Celite), solvent removal (vac.), washing (MeCN); further crop fromwashings; elem. anal.;
参考文献
Lawlor, Fiona J.; Norman, Nicholas C.; Pickett, Nigel L.; Robins, Edward G.; Nguyen, Paul; Lesley, Gerry; Marder, Todd B.; Ashmore, Jennifer A.; Green, Jennifer C.
Inorganic Chemistry, 1998 , vol. 37, # 20 p. 5282 - 5288
