1-苯基-1-三甲基甲硅氧基乙烯合成路线 (共 431 条)
反应条件
tetrakis(triphenylphosphine) palladium(0); 1,1,1,2,2,2-hexabutyl-distannane in 1,2,3,4-tetrahydro-naphthalene T=80°C; 20 h;
参考文献
Kosugi, Masanori; Koshiba, Mamoru; Sano, Hiroshi; Migita, Toshihiko
Bulletin of the Chemical Society of Japan, 1985 , vol. 58, # 3 p. 1075 - 1076
反应条件
palladium dichloride; phosphorous acid trimethyl ester in benzene T=80°C; 5 h;
参考文献
Kosugi, Masanori; Ohya, Takao; Migita, Toshihiko
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 11 p. 3539 - 3540
反应条件
[(C5Me5)Rh(vinyltrimethylsilane)2] in cyclohexane T=120°C; 72 h; Yield givenYields of byproduct given;
参考文献
Journal of the American Chemical Society, , vol. 121, # 28 p. 6616 - 6623
反应条件
potassium cyanide; 18-crown-6 ether in tetrahydrofuran 24 h; Ambient temperature;
参考文献
Gostevskii, B. A.; Kruglaya, O. A.; Albanov, A. I.; Vyazankin, N. S.
Journal of Organometallic Chemistry, 1980 , vol. 187, # 2 p. 157 - 166
反应条件
trifluorormethanesulfonic acid T=0°C; 0.5 h;
参考文献
Aizpurua, Jesus M.; Palomo, Claudio; Palomo, Antonio L.
Canadian Journal of Chemistry, 1984 , vol. 62, p. 336 - 340
反应条件
in dichloromethane T=90°C; 20 h;
参考文献
Russian Journal of General Chemistry, , vol. 75, # 5 p. 827 - 828
反应条件
tetrakis(triphenylphosphine) palladium(0); hexamethyl-silane in benzene T=100°C; 12 h;
参考文献
Journal of Organometallic Chemistry, , vol. 234, # 3 p. 367 - 374
反应条件
1: CuI / diethyl ether / -78 deg C up to 0 deg C 2: 2.) Et3N / 1.) trimethylsilyltriflate (Me3SiOTf) / 1.) pentane, RT, 1 min View Scheme
参考文献
Chemistry Letters, , p. 1967 - 1968
参考文献
Journal of Organometallic Chemistry, , vol. 11, p. 35 - 48
反应条件
lithium boron tetrafluoride in tetrahydrofuran T=20°C; 1 h;
参考文献
Tetrahedron, , vol. 49, # 37 p. 8343 - 8358