1-(2-噻吩基)-1-丙酮合成路线 （共 28 条）
反应条件
phosphorous pentoxide; phosphoric acid T=95 - 100°C; 8 h;
参考文献
Zhang, Shuguang; Huang, Shuang; Feng, Chengliang; Cai, Jin; Chen, Junqing; Ji, Min
Journal of Chemical Research, 2013 , vol. 37, # 7 p. 406 - 408
反应条件
tert.-butylhydroperoxide; tetrabutyl-ammonium chloride; sodium carbonate; copper dichloride; BQC in water T=20°C; 24 h;
参考文献
Boudreau, Josee; Doucette, Mike; Ajjou, Abdelaziz Nait
Tetrahedron Letters, 2006 , vol. 47, # 11 p. 1695 - 1698
反应条件
zinc trifluoromethanesulfonate in nitromethane T=20°C; Friedel-Crafts acylation; 4 h;
参考文献
He, Fei; Wu, Huayue; Chen, Jiuxi; Su, Weike
Synthetic Communications, 2008 , vol. 38, # 2 p. 255 - 264
反应条件
Cp*RuCl(Ph2P(CH2)2NH2-κ2-P,N); potassium tert-butylate in toluene T=30°C; 1 h;
参考文献
Ito, Masato; Kitahara, Sachiko; Ikariya, Takao
Journal of the American Chemical Society, 2005 , vol. 127, # 17 p. 6172 - 6173
反应条件
trifluoromethanesulfonic acid 2-pyridinyl ester; trifluoroacetic acid 4 h; Heating;
参考文献
Keumi, Takashi; Yoshimura, Kiichiro; Shimada, Masakazu; Kitajima, Hidehiko
Bulletin of the Chemical Society of Japan, 1988 , vol. 61, p. 455 - 460
反应条件
1: 84 percent / tetrahydrofuran 2: 99 percent Spectr. / Cp*RuCl[Ph2P(CH2)2NH2-κ2-P,N]; t-BuOK / toluene / 1 h / 30 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 127, # 17 p. 6172 - 6173
参考文献
Journal of the American Chemical Society, , vol. 69, p. 3093,3095
反应条件
tin(IV) chloride; benzene Behandeln des Reaktionsgemisches mit Wasser;
参考文献
Zhurnal Obshchei Khimii, , vol. 29, p. 3873,3878; engl. Ausg. S. 3831, 3836
参考文献
Bulletin de la Societe Chimique de France, , vol. <4> 23, p. 291
反应条件
alkaline permanganate
参考文献
Krekeler
Chemische Berichte, 1886 , vol. 19, p. 677
Full Text Show Details
Curtius; Thyssen
Journal fuer Praktische Chemie (Leipzig), 1902 , vol. <2> 65, p. 6
