N-环己基-4-硝基苯胺合成路线 (共 14 条)
反应条件
potassium carbonate in water T=100°C; Ullmann Condensation; 1 h; Sealed tubeMicrowave irradiation;
参考文献
Nasir Baig; Varma, Rajender S.
RSC Advances, 2014 , vol. 4, # 13 p. 6568 - 6572
反应条件
potassium carbonate in N,N-dimethyl-formamide T=100°C; 8 h;
参考文献
Sreedhar; Arundhathi; Linga Reddy; Amarnath Reddy; Lakshmi Kantam
Synthesis, 2009 , # 15 art. no. P03909SS, p. 2517 - 2522
反应条件
oxygen; triethylamine; [Cu3(1,3,5-benzenetricarboxylate)2] in dichloromethane T=20°C; 5 h; Product distribution / selectivity;
参考文献
THE REGENTS OF THE UNIVERSITY OF CALIFORNIA; BASF SE; YAGHI, Omar, M.; CZAJA, Alexander, U.; WANG, Bo; LU, Zheng
Patent: WO2011/14503 A1, 2011 ;
Location in patent: Page/Page column 23-28 ;
反应条件
potassium tert-butylate in dimethyl sulfoxide 0.25 h; Ambient temperature;
参考文献
Katritzky, Alan R.; Laurenzo, Kathleen S.
Journal of Organic Chemistry, 1988 , vol. 53, # 17 p. 3978 - 3982
反应条件
sodium tris(acetoxy)borohydride; acetic acid in 1,2-dichloro-ethane T=140°C; 0.166667 h; microwave irradiation;
参考文献
Bailey, Helen V.; Heaton, Wesley; Vicker, Nigel; Potter, Barry V. L.
Synlett, 2006 , # 15 p. 2444 - 2448
反应条件
[BsTmG][CF3COO] in 1,4-dioxane T=140°C; 24 h;
参考文献
Han, Feng; Yang, Lei; Li, Zhen; Xia, Chungu
Advanced Synthesis and Catalysis, 2012 , vol. 354, # 6 p. 1052 - 1060
反应条件
in dimethyl sulfoxide; nitrobenzene
参考文献
Monsanto Company
Patent: US5252737 A1, 1993 ;
反应条件
polymethylhydrosiloxane in dichloromethane T=20°C;
参考文献
Patel, Jay P.; Li, An-Hu; Dong, Hanqing; Korlipara, Vijaya L.; Mulvihill, Mark J.
Tetrahedron Letters, 2009 , vol. 50, # 44 p. 5975 - 5977
反应条件
silver hexafluoroantimonate; 1,2-bis-(diphenylphosphino)ethane; copper(ll) bromide in tetrachloroethane, 1,1,2,2- T=100°C; 48 h; Inert atmosphere;
参考文献
Michon, Christophe; Medina, Florian; Capet, Frederic; Roussel, Pascal; Agbossou-Niedercorn, Francine
Advanced Synthesis and Catalysis, 2010 , vol. 352, # 18 p. 3293 - 3305
反应条件
acetone in pyridine T=70°C; 3 h;
参考文献
Tohda, Yasuo; Ariga, Masahiro; Kawashima, Toshihide; Matsumura, Eizo
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 1 p. 201 - 204