反应条件
n-butyllithium; N,N,N',N,-tetramethylethylenediamine; potassium tert-butylate
1.) hexane, from -20 deg C to 10 deg C, 1.5 h, 2.) THF, 30 - 35 deg C, 30 min; Yield given. Multistep reaction;
参考文献
Andringa, H.; Verkruijsse, H.D.; Brandsma, L.; Lochmann, L.
Journal of Organometallic Chemistry, 1990 , vol. 393, # 3 p. 307 - 314