N,N-二乙基-2-萘甲酰胺合成路线 （共 6 条）
反应条件
(η5-cyclopentadienyl)2TiF2; methylphenylsilane in toluene T=20°C; Title compound not separated from byproducts;
参考文献
Angewandte Chemie - International Edition, , vol. 40, # 11 p. 2129 - 2131
反应条件
N,N,N',N,-tetramethylethylenediamine; sec.-butyllithium in diethyl ether 1.) -78 deg C, 1 h, 2.) -78 deg C -> RT, 12 h;
参考文献
Journal of the American Chemical Society, , vol. 102, # 4 p. 1457 - 1460
反应条件
1: With disodium hydrogenphosphate in acetonitrile T=20°C; Methylation; 2: With sodium hydrogencarbonate Hydrolysis; 18 h;
参考文献
Keck, Gary E; McLaws, Mark D; Wager, Travis T
Tetrahedron, 2000 , vol. 56, # 51 p. 9875 - 9883
反应条件
pyridine; trifluoromethylsulfonic anhydride 1.) CH2Cl2, -40 to 0 deg C, 2 h; 0 deg C, 10 h, 2.) r.t., 12 h; Yield given. Multistep reaction;
参考文献
Charette, Andre B.; Chua, Peter
Synlett, 1998 , # 2 p. 163 - 165
反应条件
(η5-cyclopentadienyl)2TiF2; methylphenylsilane in toluene T=80°C;
参考文献
Rangareddy, Kesamreddy; Selvakumar, Kumaravel; Harrod, John F.
Journal of Organic Chemistry, 2004 , vol. 69, # 20 p. 6843 - 6850
反应条件
(η5-cyclopentadienyl)2TiF2; methylphenylsilane in toluene T=20°C; Title compound not separated from byproducts;
参考文献
Rangareddy, Kesamreddy; Selvakumar, Kumaravel; Harrod, John F.
Journal of Organic Chemistry, 2004 , vol. 69, # 20 p. 6843 - 6850
