N-叔丁氧羰基-L-谷氨酸5-苄酯合成路线 （共 35 条）
参考文献
Justus Liebigs Annalen der Chemie, , vol. 673, p. 196 - 207
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 1523 - 1526
反应条件
bis(trichloromethyl) carbonate; triethylamine in ethyl acetate Ambient temperature;
参考文献
Wilder, Renee; Mobashery, Shahriar
Journal of Organic Chemistry, 1992 , vol. 57, # 9 p. 2755 - 2756
反应条件
1: 94 percent / DCC, pyridine / ethyl acetate / Ambient temperature 2: 99 percent / H2 / 10percent Pd/C / methanol / 2 h View Scheme
参考文献
Robin, Sylvie; Zhu, Jiarong; Galons, Herve; Pham-Huy, Chuong; Claude, Jean Roger; et al.
Tetrahedron: Asymmetry, 1995 , vol. 6, # 6 p. 1249 - 1252
反应条件
Nafion H; dimethylsulfide; 3-methyl-phenol; trifluoroacetic acid 3 h;
参考文献
Tam, James P.; Heath, William F.; Merrifield, R. B.
Tetrahedron Letters, 1982 , vol. 23, # 43 p. 4435 - 4438
反应条件
ammonia; triethylamine in tetrahydrofuran; methanol; water
参考文献
Ajinomoto Co., Inc.; YASUDA Reiko; ETO Yuzuru; KITAHARA Yoshiro
Patent: EP2543660 A1, 2013 ;
Location in patent: Paragraph 0123 ;
反应条件
1: 4-(N,N-dimethlyamino)pyridine / dichloromethane / 12 h / 20 °C 2: hydrogen; 10 Pd/C / dichloromethane; methanol / 12 h / 20 °C / 760.05 Torr View Scheme
参考文献
Tian, Xizhe; Pai, Jaeyoung; Shin, Injae
Chemistry - An Asian Journal, 2012 , vol. 7, # 9 p. 2052 - 2060
反应条件
magnesium; hydrazinium monoformate in methanol T=25°C; 1 h;
参考文献
Tetrahedron Letters, , vol. 43, # 2 p. 311 - 313
反应条件
dicyclohexyl-carbodiimide in ethylene glycol dimethyl ether T=5°C; 18 h;
参考文献
Hoekstra, William J.; Sunder, Shyam S.; Cregge, Robert J.; Ashton, Louis A.; Stewart, Kenneth T.; King, Chi-Hsin R.
Tetrahedron, 1992 , vol. 48, # 2 p. 307 - 318
反应条件
dicyclohexyl-carbodiimide in 1,4-dioxane; ethyl acetate T=0°C; 2 h;
参考文献
Gisin, B.F.; Davis, D.G.; Borowska, Z.K.; Hall, J.E.; Kobayashi, S.
Journal of the American Chemical Society, 1981 , vol. 103, # 21 p. 6373 - 6377
