in neat (no solvent) reaction in a melting tube at about 200-250°C;;
参考文献
Besson, A.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1891 , vol. 112, p. 1447 - 1449
Full Text Show Details
Gmelin Handbook: Si: MVol.B, 275, page 742 - 743
in neat (no solvent) reaction near red heat; small yields only;;
参考文献
Besson, A.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1891 , vol. 112, p. 1447 - 1449
Full Text Show Details
Gmelin Handbook: Si: MVol.B, 275, page 742 - 743
in neat (no solvent) byproducts: SiBr4; distillation of a solution of I2 and SiBr4 or passing the mixture in a H2 stream to crystalline Si near red heat;;
参考文献
Besson, A.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1891 , vol. 112, p. 1447 - 1449
Full Text Show Details
Gmelin Handbook: Si: MVol.B, 275, page 742 - 743
in neat (no solvent) distillation of BrI or passing BrI in a H2 stream to crystalline Si near red heat;;
参考文献
Besson, A.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1891 , vol. 112, p. 1447 - 1449
Full Text Show Details
Gmelin Handbook: Si: MVol.B, 275, page 742 - 743
