2-(三甲基硅基)-1,2,3-三氮唑合成路线 (共 6 条)
反应条件
triethylamine in benzene T=80°C; 2 h;
参考文献
Ohta, Shunsaku; Kawasaki, Ikuo; Uemura, Takahiro; Yamashita, Masayuki; Yoshioka, Tomomichi; Yamaguchi, Satoshi
Chemical and Pharmaceutical Bulletin, 1997 , vol. 45, # 7 p. 1140 - 1145
反应条件
6 h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Magnetic Resonance in Chemistry, , vol. 36, # 2 p. 110 - 115
反应条件
T=140°C; Condensation; 3 h;
参考文献
Journal of Medicinal Chemistry, , vol. 43, # 16 p. 3111 - 3117
反应条件
tetrabutyl ammonium fluoride in acetonitrile T=80°C; 2 h; other alkyl halide, also with MeOCH2Cl and PhCOCH2Br, var. temp. var. time; Product distribution;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 45, # 7 p. 1140 - 1145
反应条件
tetrabutyl ammonium fluoride in acetonitrile
12 h; Heating;
参考文献
Ohta, Shunsaku; Kawasaki, Ikuo; Uemura, Takahiro; Yamashita, Masayuki; Yoshioka, Tomomichi; Yamaguchi, Satoshi
Chemical and Pharmaceutical Bulletin, 1997 , vol. 45, # 7 p. 1140 - 1145
反应条件
in sulfolane
T=140°C; 3 h;
参考文献
Williams, Eric L.
Tetrahedron Letters, 1992 , vol. 33, # 8 p. 1033 - 1036