in neat (no solvent) form of SiCl4 and molten KI;;
参考文献
Forbes, G. S.; Anderson, H. H.
Journal of the American Chemical Society, 1944 , vol. 66, p. 931 - 933
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Gmelin Handbook: Si: MVol.B, 275, page 742 - 743
pyridium iodide in chloroform to the soln. of SiI2Cl2/CHCl3 the soln. of pyridinium iodide/CHCl3 was added dropwise with stirring, refluxed for 8 h at 334 K under protectivegas; gas chromy.;
参考文献
Hass, D.; Bechstein, O.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1981 , vol. 483, p. 140 - 144
pyridine hydrochloride in chloroform to the soln. of SiI4/CHCl3 the soln. of pyridinium chloride/CHCl3 was added dropwise with stirring, stirred at 298°C under protective gas; gas chromy.;
参考文献
Hass, D.; Bechstein, O.
Zeitschrift fuer Anorganische und Allgemeine Chemie, 1981 , vol. 483, p. 140 - 144
on distilling of compd. on iodine and storing at room temp.;; about half of amt. (compd.) is still unchanged, some amt. is reacting to Cl3SII and a black ppt. is resting (distn. not possible);;
in neat (no solvent) heating of SiHCl3 and I2 in a melting tube at 200 -250°C;;
参考文献
Besson, A.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1891 , vol. 112, p. 611 - 614
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Gmelin Handbook: Si: MVol.B, 275, page 742 - 743
in neat (no solvent) distillation of ICl to crystalline Si near red heat;; fractional distillation over Cu filings;;
参考文献
Besson, A.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1891 , vol. 112, p. 1314 - 1316
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Gmelin Handbook: Si: MVol.B, 275, page 742 - 743
in neat (no solvent) passing SiCl4 vapors with HI through a glass tube at red heat;;
参考文献
Besson, A.
Comptes Rendus Hebdomadaires des Seances de l'Academie des Sciences, 1891 , vol. 112, p. 611 - 614
Full Text Show Details
Gmelin Handbook: Si: MVol.B, 275, page 742 - 743
