in neat (no solvent)
absence of air and moisture; 150 mbar Br2, 320 mbar NO, 20°C, 30 min; fractional condensation at -65, -120, -196°C (product in -120°C trap);
sulfuric acid
Kinetics; byproducts: H2O; heterogeneous reaction of components on aq. H2SO4 (40-95 wt.-percent) in Knudsen flow reactor in temp. range 180-200 K;
参考文献
Seisel, Sabine; Rossi, Michel J.
Berichte der Bunsengesellschaft/Physical Chemistry Chemical Physics, 1997 , vol. 101, # 6 p. 943 - 955
in neat (no solvent)
reaction at high temperatures;;
参考文献
Johnson, C. R.; Nunn, L. G.
Journal of the American Chemical Society, 1941 , vol. 63, p. 141 - 143
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Gmelin Handbook: P: MVol.C, 215, page 494 - 496
