1,1-二氟-2-苯基环丙烷合成路线 (共 11 条)
反应条件
tetrabutyl-ammonium chloride in tetrahydrofuran T=110°C; [2+1] cycloaddition; 4 h;
参考文献
Wang, Fei; Zhang, Wei; Zhu, Jieming; Li, Huaifeng; Huang, Kuo-Wei; Hu, Jinbo
Chemical Communications, 2011 , vol. 47, # 8 p. 2411 - 2413
反应条件
sodium iodide in tetrahydrofuran T=65°C; 2 h; Inert atmosphere;
参考文献
Wang, Fei; Luo, Tao; Hu, Jinbo; Wang, Ying; Krishnan, Hema S.; Jog, Parag V.; Ganesh, Somesh K.; Prakash, G. K. Surya; Olah, George A.
Angewandte Chemie - International Edition, 2011 , vol. 50, # 31 p. 7153 - 7157
反应条件
α-[2-(2-butoxyethoxy)ethoxy]-4,5-methylenedioxy-2-propyltoluene; tetrabutylammomium bromide in 1,2-dichloro-ethane T=70°C; 30 h;
参考文献
Fritz, Heinz P.; Kornrumpf, Wolfgang
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1981 , vol. 36, # 11 p. 1375 - 1380
反应条件
aluminium trichloride in acetonitrile T=-20°C; 1 h;
参考文献
Kirii; Pazenok; Yagupolskii; Naumann; Turra
Russian Journal of Organic Chemistry, 2001 , vol. 37, # 2 p. 207 - 209
反应条件
2,2'-azo-bisisobutyronitrile in N,N-dimethyl-formamide 6 h; Heating;
参考文献
Chang, Ying; Cai, Chun
Chemistry Letters, 2005 , vol. 34, # 10 p. 1440 - 1441
参考文献
Moss,R.A.; Mallon,C.B.
Journal of the American Chemical Society, 1975 , vol. 97, # 2 p. 344 - 347
反应条件
sodium iodide in ethylene glycol dimethyl ether
参考文献
Seyferth,D. et al.
Journal of Organic Chemistry, 1967 , vol. 32, p. 2980 - 2984
反应条件
oxirane; tetrabutyl-ammonium chloride
参考文献
Kamel,M. et al.
Chemische Berichte, 1976 , vol. 109, p. 2351 - 2369
反应条件
in tetrahydrofuran T=-70°C;
参考文献
Suda, Minoru
Tetrahedron Letters, 1980 , vol. 21, p. 4355 - 4358
反应条件
hydrogen; Trimethylene glycol in methanol P=760 Torr; Ambient temperaturevar. catalysts, var. bases, var times; Product distribution;
参考文献
Isogai; Nishizawa; Saito; Sakai
Bulletin of the Chemical Society of Japan, 1983 , vol. 56, # 5 p. 1555 - 1556