1-二氯磷酰-3-甲基-丁-1,2-二烯合成路线 （共 9 条）
反应条件
phosphorus trichoride in dichloromethane
参考文献
Enchev
Phosphorus, Sulfur and Silicon and the Related Elements, 2008 , vol. 183, # 11 p. 2649 - 2654
反应条件
triethylamine in tetrachloromethane 2 h; Heating;
参考文献
Mikhailova, T. S.; Ignat'ev, V. M.; Ionin, B. I.; Petrov, A. A.
J. Gen. Chem. USSR (Engl. Transl.), 1980 , vol. 50, # 4 p. 762 - 770,605 - 611
反应条件
sodium hydrogencarbonate
参考文献
Macomber,R.S.; Kennedy,E.R.
Journal of Organic Chemistry, 1976 , vol. 41, p. 3191 - 3197
反应条件
in dichloromethane 1.) 0 deg C, 45 min, 2.) r.t., 3 h; Yield given;
参考文献
Linden, Johannes B. van der; Lucassen, Andre C. B.; Zwanenburg, Binne
Recueil des Travaux Chimiques des Pays-Bas, 1994 , vol. 113, # 12 p. 547 - 551
反应条件
in benzene T=80 - 90°C; 15 h;
参考文献
Russian Journal of General Chemistry, , vol. 71, # 3 p. 339 - 342
反应条件
magnesium in diethyl ether
参考文献
Angelov, Christo M.; Enchev, Dobromir D.
Phosphorus and Sulfur and the Related Elements, 1988 , vol. 37, p. 125 - 128
反应条件
diisopropyl phosphonesulfenyl chloride in tetrachloromethane
Ambient temperature;
参考文献
Khusainova, N. G.; Naumova, L. V.; Berdnikov, E. A.; Kutyrev, G. A.; Pudovik, A. N.
Phosphorus and Sulfur and the Related Elements, 1982 , vol. 13, p. 147 - 152
反应条件
1: aq. NaHCO3
2: aq. HCl
View Scheme
参考文献
Macomber,R.S.; Kennedy,E.R.
Journal of Organic Chemistry, 1976 , vol. 41, p. 3191 - 3197
反应条件
1: Cl2 / CCl4
2: Py / diethyl ether
3: H2 / Pd-C / ethanol
View Scheme
参考文献
Angelov,Kh.M. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1978 , vol. 48, p. 1487 - 1495,1365 - 1371
