1-叔丁基-4-亚甲基环己烷合成路线 （共 50 条）
参考文献
Bordwell,F.G. et al.
Journal of Organic Chemistry, 1965 , vol. 30, p. 3764 - 3768
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Carlson,R.G.; Behn,N.S.
Journal of Organic Chemistry, 1967 , vol. 32, p. 1363 - 1367
反应条件
(i), (ii) MeSO2Cl, Et3N, CH2Cl2; Multistep reaction;
参考文献
Reich,H.J.; Chow,F.
Journal of the Chemical Society, Chemical Communications, 1975 , p. 790 - 791
反应条件
in toluene
24 h; var. molar ratio of reagents, var. solvents; other ketones, other alanes; Product distributionMechanism;
参考文献
Ashby, E. C.; Smith, R. Scott
Journal of Organometallic Chemistry, 1982 , vol. 225, # 1 p. 71 - 85
反应条件
α-hydroperoxy-α-methoxyacetophenone; oxygen in dichloromethane
T=25°C; 20 h;
参考文献
Yamamoto, Hiroshi; Miura, Masahiro; Nojima, Masatomo; Kusabayashi, Shigekazu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 173 - 182
反应条件
oxygen in dichloromethane
T=25°C; 20 h;
参考文献
Yamamoto, Hiroshi; Miura, Masahiro; Nojima, Masatomo; Kusabayashi, Shigekazu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 173 - 182
反应条件
oxygen in dichloromethane
T=25°C; 20 h; other reagents, temperature and time; Product distribution;
参考文献
Yamamoto, Hiroshi; Miura, Masahiro; Nojima, Masatomo; Kusabayashi, Shigekazu
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 173 - 182
反应条件
1: N-bromoacetamide, CH3COONa / acetone; H2O / 10 h / Ambient temperature
2: 90 percent / 5 percent KOH / methanol / Ambient temperature
3: 6 percent / H2 / Ni Raney / cyclohexane / 20 °C / 760 Torr
View Scheme
参考文献
Accrombessi, Georges; Geneste, Patrick; Olive, Jean-Louis; Pavia, Andre Armand
Bulletin de la Societe Chimique de France, 1981 , vol. 2, # 1-2 p. 19 - 23
反应条件
iodine in benzene
17.5 h; Ambient temperatureIrradiation; Further byproducts given. Yields of byproduct given;
参考文献
Cambie, Richard C.; Rutledge, Peter S.; Strange, Gary A.; Woodgate, Paul D.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 553 - 565
反应条件
iodine in benzene
18 h; Irradiationother temperature; Product distribution;
参考文献
Cambie, Richard C.; Rutledge, Peter S.; Strange, Gary A.; Woodgate, Paul D.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 553 - 565
反应条件
Lit.: Kopecky, K.R. et al.; Can.J.Chem. 1975, 53, 1103;
参考文献
Baumstark, Alfons L.; Niroomand, Farhad; Vasquez, Pedro C.
Journal of Organic Chemistry, 1984 , vol. 49, # 23 p. 4497 - 4500
