1,1,1,5,5,5-六氟-2,4-二(三氟甲基)-2,3-戊二烯合成路线 (共 11 条)
反应条件
cesium fluoride in diethylene glycol dimethyl ether T=20°C; 1.5 h;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 30, # 7 p. 1350 - 1352
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 7 p. 1661 - 1663
反应条件
T=600°C; P=1 - 5 Torr;
参考文献
Journal of the American Chemical Society, , vol. 88, p. 5582 - 5587
参考文献
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , p. 2563 - 2566
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , p. 2772 - 2775
C.A., , vol. 90, p. 120923
F: PerFHalOrg.SVol.1, 1.3, page 16 - 19
反应条件
mercury 175 h; Irradiationin vacuo (sealed tube);
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 7 p. 2080 - 2086
反应条件
T=500°C; various reaction conditions; Product distribution;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 35, # 6 p. 1217 - 1219
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 6 p. 1341 - 1344
反应条件
cesium fluoride 1.) diglyme; 2.) 12 h, 20 deg C; Multistep reaction. Title compound not separated from byproducts;
参考文献
Volkonsky,A.Y.; Rokhlin,E.M.
Journal of Fluorine Chemistry, 1984 , vol. 26, p. 183
反应条件
T=1000°C; P=760 Torr; Product distributionMechanism;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 39, # 11 p. 2408 - 2410
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 11 p. 2655 - 2657
反应条件
T=1000°C; P=760 Torr; Product distributionMechanism;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 39, # 11 p. 2408 - 2410
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 11 p. 2655 - 2657
反应条件
T=1000°C; P=760 Torr; Product distributionMechanism;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 39, # 11 p. 2408 - 2410
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 11 p. 2655 - 2657
反应条件
T=1000°C; P=760 Torr; Product distributionMechanism;
参考文献
Kagramanov, N. D.; Kutin, A.A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990 , vol. 39, # 11 p. 2408 - 2410
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990 , # 11 p. 2655 - 2657