N-乙基-2-甲基-1-丙胺合成路线 (共 9 条)
反应条件
hydrogen in ethylene glycol dimethyl ether T=160°C; P=22502.3 Torr; 20 h; Inert atmosphereAutoclaveMolecular sieve;
参考文献
Stein, Mario; Breit, Bernhard
Angewandte Chemie - International Edition, 2013 , vol. 52, # 8 p. 2231 - 2234
反应条件
ethanol anschliessenden Hydrierung an Platin;
参考文献
Smirnov, Yu. D.; Pavlichenko, V. F.; Tomilov, A. P.
Journal of Organic Chemistry USSR (English Translation), 1992 , vol. 28, # 3.1 p. 374 - 380
Zhurnal Organicheskoi Khimii, 1992 , vol. 28, # 3 p. 461 - 467
反应条件
1: With diisobutylaluminium hydride in tetrahydrofuran; hexane; dichloromethane T=0 - 20°C; 2 h; Inert atmosphere; 2: With water; NAF in tetrahydrofuran; hexane; dichloromethane T=0°C; 0.5 h; Inert atmosphere; regioselective reaction;
参考文献
Cho, Hidetsura; Iwama, Yusuke; Sugimoto, Kenji; Mori, Seiji; Tokuyama, Hidetoshi
Journal of Organic Chemistry, 2010 , vol. 75, # 3 p. 627 - 636
反应条件
supercritical CO2; hydrogen; 4-H2F8-TPP; (hexafluoroacetylacetonato)(1,5-cyclooctadiene)rhodium(I) T=78°C; P=30003 Torr; 20 h; Product distribution; Further Variations:PressuresTemperaturestime;
参考文献
Wittmann, Klaus; Wisniewski, Wolfgang; Mynott, Richard; Leitner, Walter; Kranemann, Christian Ludger; Rische, Thorsten; Eilbracht, Peter; Kluwer, Sander; Ernsting, Jan Meine; Elsevier, Cornelis J.
Chemistry - A European Journal, 2001 , vol. 7, # 21 p. 4584 - 4589
反应条件
hydrogenchloride in tetrahydrofuran
参考文献
Zwierzak,A.; Podstawczynska,I.
Angewandte Chemie, 1977 , vol. 89, p. 737 - 738
参考文献
Shares, Jonathan; Yehl, Jenna; Kowalsick, Amanda; Byers, Philip; Haaf, Michael P.
Tetrahedron Letters, 2012 , vol. 53, # 33 p. 4426 - 4428
反应条件
in xylene 6 h; Heating;
参考文献
Brown, Herbert C.; Midland, M. Mark; Levy, Alan B.
Tetrahedron, 1987 , vol. 43, # 18 p. 4079 - 4088
参考文献
Cope et al.
Journal of the American Chemical Society, 1957 , vol. 79, p. 4720,4727
参考文献
Marckwald; v.Droste-Huelshoff
Chemische Berichte, 1899 , vol. 32, p. 562