(三甲基硅基)甲基氯化镁合成路线 （共 130 条）
反应条件
1: in diethyl ether T=0 - 20°C; 2: With anhydrous iron chloride; ethylmagnesium bromide in diethyl ether T=0 - 20°C;
参考文献
Creary, Xavier; Kochly, Elizabeth D.
Journal of Organic Chemistry, 2009 , vol. 74, # 5 p. 2134 - 2144
反应条件
in tetrahydrofuran
0.5 h; Ambient temperature;
参考文献
Fuerstner, Alois; Kollegger, Gerlinde; Weidmann, Hans
Journal of Organometallic Chemistry, 1991 , vol. 414, # 3 p. 295 - 305
反应条件
in tetrahydrofuran
2 h; Ambient temperature;
参考文献
Fuerstner, Alois; Kollegger, Gerlinde; Weidmann, Hans
Journal of Organometallic Chemistry, 1991 , vol. 414, # 3 p. 295 - 305
反应条件
in tetrahydrofuran
0.5 h; Ambient temperature;
参考文献
Fuerstner, Alois; Kollegger, Gerlinde; Weidmann, Hans
Journal of Organometallic Chemistry, 1991 , vol. 414, # 3 p. 295 - 305
反应条件
CoCl2 in tetrahydrofuran
T=25°C; 12 h;
参考文献
Affo, Walter; Ohmiya, Hirohisa; Fujioka, Takuma; Ikeda, Yousuke; Nakamura, Tomoaki; Yorimitsu, Hideki; Oshima, Koichiro; Imamura, Yuki; Mizuta, Tsutomu; Miyoshi, Katsuhiko
Journal of the American Chemical Society, 2006 , vol. 128, # 24 p. 8068 - 8077
反应条件
1:
2: Pummerer Sulfoxide Rearrangement; 5 h; Reflux; Temperature;
参考文献
Mikina, Maciej
Phosphorus, Sulfur and Silicon and the Related Elements, 2013 , vol. 188, # 4 p. 454 - 458
参考文献
Leigh, William J.; Boukherroub, Rabah; Kerst, Corinna
Journal of the American Chemical Society, 1998 , vol. 120, # 37 p. 9504 - 9512
反应条件
boron trifluoride diethyl etherate
参考文献
Seyferth
Journal of the American Chemical Society, 1959 , vol. 81, p. 1844,1846
Full Text Show Details
Dow Corning Corp.
Patent: US2831009 , 1956 ;
反应条件
CoCl2 in tetrahydrofuran; diethyl ether
T=-20°C;
参考文献
Ohmiya, Hirohisa; Yorimitsu, Hideki; Oshima, Koichiro
Angewandte Chemie - International Edition, 2005 , vol. 44, # 22 p. 3488 - 3490
反应条件
bis(acetylacetonate)nickel(II) in diethyl ether
Ambient temperature;
参考文献
Sengupta, Saumitra; Leite, Magda; Raslan, Delio Soares; Quesnelle, Claude; Snieckus, Victor
Journal of Organic Chemistry, 1992 , vol. 57, # 15 p. 4066 - 4068
