1-羟基-1,2-苯碘酰-3(1H)-酮合成路线 （共 44 条）
反应条件
di-tert-butyl peroxide; boron trifluoride diethyl etherate in chloroform T=0°C; 3 h;
参考文献
Ochiai, Masahito; Ito, Takao; Takahashi, Hideo; Nakanishi, Akinobu; Toyonari, Mika; Sueda, Takuya; Goto, Satoru; Shiro, Motoo
Journal of the American Chemical Society, 1996 , vol. 118, # 33 p. 7716 - 7730
反应条件
in water T=20°C; Suzuki reaction;
参考文献
Yan, Jie; Jin, Hongwei; Shan, Shang
Tetrahedron, 2006 , vol. 62, # 24 p. 5603 - 5607
反应条件
1: With palladium diacetate in N,N-dimethyl-formamide T=60°C; Addition; 3 h; 2: With hydrogenchloride in N,N-dimethyl-formamide T=20°C; Hydrolysis;
参考文献
Xia, Min; Chen, Zhenchu
Synthetic Communications, 2000 , vol. 30, # 1 p. 63 - 68
反应条件
1: With palladium diacetate in N,N-dimethyl-formamide T=60°C; Addition; 3 h; 2: With hydrogenchloride in N,N-dimethyl-formamide T=20°C; Hydrolysis;
参考文献
Xia, Min; Chen, Zhenchu
Synthetic Communications, 2000 , vol. 30, # 1 p. 63 - 68
反应条件
2: quinoline View Scheme
参考文献
Baker,G.P. et al.
Journal of the Chemical Society, 1965 , p. 3721 - 3728
反应条件
1.1: trimethylsilyl trifluoromethanesulfonate / acetonitrile / 0.75 h / 0 °C 1.2: 0.75 h / 0 °C 1.3: 0.25 h 2.1: sodium hydroxide / tetrahydrofuran; water / 0.08 h / 20 °C 2.2: 0.08 h / 20 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 135, # 26 p. 9620 - 9623
反应条件
1: With palladium diacetate in N,N-dimethyl-formamide T=60°C; Addition; 3 h; 2: With hydrogenchloride in N,N-dimethyl-formamide T=20°C; Hydrolysis;
参考文献
Xia, Min; Chen, Zhenchu
Synthetic Communications, 2000 , vol. 30, # 1 p. 63 - 68
反应条件
iodine; trifluoroacetic acid in acetonitrile-D3
参考文献
Brand, Jonathan P.; Waser, Jerome
Synthesis, 2012 , vol. 44, # 8 p. 1155 - 1158
反应条件
1: 0.25 h / Heating 2: 6.78 g / 0.25 h / Heating 3: 55 percent / CsF / acetonitrile / 15 h / 20 °C View Scheme
参考文献
Eisenberger, Patrick; Gischig, Sebastian; Togni, Antonio
Chemistry - A European Journal, 2006 , vol. 12, # 9 p. 2579 - 2586
反应条件
1: With palladium diacetate in N,N-dimethyl-formamide T=60°C; Addition; 3 h; 2: With hydrogenchloride in N,N-dimethyl-formamide T=20°C; Hydrolysis;
参考文献
Xia, Min; Chen, Zhenchu
Synthetic Communications, 2000 , vol. 30, # 1 p. 63 - 68
