(Z)-1,1-二乙氧基十三碳-2-烯合成路线 （共 5 条）
反应条件
C35H45N3O4Ru in tetrahydrofuran T=35°C; 3 h; stereoselective reaction;
参考文献
Quigley, Brendan L.; Grubbs, Robert H.
Chemical Science, 2014 , vol. 5, # 2 p. 501 - 506
反应条件
in diethyl ether 1.) 0 deg C, 15 min, 2.) r.t., 3 h;
参考文献
Bestmann, Hans Juergen; Roth, Kurt; Ettlinger, Manfred
Chemische Berichte, 1982 , vol. 115, # 1 p. 161 - 171
参考文献
Bestmann,H.J. et al.
Angewandte Chemie, 1979 , vol. 91, p. 748
反应条件
toluene-4-sulfonic acid in water; acetone
T=0°C; 0.25 h; Yield given. Title compound not separated from byproducts;
参考文献
Bestmann, Hans Juergen; Roth, Kurt; Ettlinger, Manfred
Chemische Berichte, 1982 , vol. 115, # 1 p. 161 - 171
反应条件
1: p-CH3-C6H4-SO3H / acetone; H2O / 0.25 h / 0 °C
2: p-CH3-C6H4-SO3H / CHCl3 / Heating
View Scheme
参考文献
Bestmann, Hans Juergen; Roth, Kurt; Ettlinger, Manfred
Chemische Berichte, 1982 , vol. 115, # 1 p. 161 - 171
