6-氯-2,2’-联吡啶合成路线 （共 19 条）
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene 11 h; Reflux;
参考文献
Shinonogi and Co., Ltd
Patent: US2011/28468 A1, 2011 ;
Location in patent: Page/Page column 22 ;
参考文献
Pornsuriyasak, Papapida; Rath, Nigam P.; Demchenko, Alexei V.
Chemical Communications, 2008 , # 43 p. 5633 - 5635
反应条件
tetrakis(triphenylphosphine) palladium(0) in xylene Condensation; 12 h; Heating;
参考文献
Choppin, Sabine; Gros, Philippe; Fort, Yves
Organic Letters, 2000 , vol. 2, # 6 p. 803 - 805
参考文献
American Cyanamid Company
Patent: US4550166 A1, 1985 ;
反应条件
trichlorophosphate 12 h; Heating;
参考文献
Araki, Koji; Mutai, Toshiki; Shigemitsu, Yasuhiro; Yamada, Masaki; Nakajima, Takayoshi; et al.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1996 , # 4 p. 613 - 618
反应条件
phosphorus pentachloride; trichlorophosphate T=130°C; 3 h;
参考文献
Field, John S.; Haines, Raymond J.; Parry, Campbell J.; Sookraj, Sadesh H.
South African Journal of Chemistry, 1993 , vol. 46, # 3/4 p. 70 - 74
反应条件
1: With methyl iodide in nitrobenzene 2: With sodium hydroxide; potassium hexacyanoferrate(III) 3: With phosphorus pentachloride; phosphorus trichoride
参考文献
Wang, Fen; Schwabacher, Alan W.
Tetrahedron Letters, 1999 , vol. 40, # 26 p. 4779 - 4782
反应条件
1: EtMgBr / tetrahydrofuran / 0.42 h / Ambient temperature 2: 43 percent / tetrahydrofuran / 3 h / Ambient temperature View Scheme
参考文献
Furukawa, Naomichi; Shibutani, Tadao; Fujihara, Hisashi
Tetrahedron Letters, 1987 , vol. 28, # 47 p. 5845 - 5848
反应条件
in tetrahydrofuran 3 h; Ambient temperature;
参考文献
Furukawa, Naomichi; Shibutani, Tadao; Fujihara, Hisashi
Tetrahedron Letters, 1987 , vol. 28, # 47 p. 5845 - 5848
反应条件
Multistep reaction.;
参考文献
Gros, Philippe; Doudouh, Abdelatif; Fort, Yves
Tetrahedron Letters, 2004 , vol. 45, # 33 p. 6239 - 6241
