S-(三氟甲基)二苯并噻吩三氟甲基磺酸盐合成路线 (共 67 条)
反应条件
2,4,6-trimethyl-pyridine; copper diacetate in N,N-dimethyl acetamide T=25°C; P=760.051 Torr; 16 h; Inert atmosphere;
参考文献
Xu, Jun; Luo, Dong-Fen; Xiao, Bin; Liu, Zhao-Jing; Gong, Tian-Jun; Fu, Yao; Liu, Lei
Chemical Communications, 2011 , vol. 47, # 14 p. 4300 - 4302
反应条件
2,4,6-trimethyl-pyridine; copper diacetate in N,N-dimethyl acetamide T=0°C; P=760.051 Torr; 16 h; Inert atmosphere;
参考文献
Xu, Jun; Luo, Dong-Fen; Xiao, Bin; Liu, Zhao-Jing; Gong, Tian-Jun; Fu, Yao; Liu, Lei
Chemical Communications, 2011 , vol. 47, # 14 p. 4300 - 4302
反应条件
2,4,6-trimethyl-pyridine; copper diacetate in N,N-dimethyl acetamide T=25°C; P=760.051 Torr; 16 h; Inert atmosphere;
参考文献
Xu, Jun; Luo, Dong-Fen; Xiao, Bin; Liu, Zhao-Jing; Gong, Tian-Jun; Fu, Yao; Liu, Lei
Chemical Communications, 2011 , vol. 47, # 14 p. 4300 - 4302
反应条件
in N,N-dimethyl-formamide T=80°C; 5 h; Title compound not separated from byproducts;
参考文献
Tetrahedron Letters, , vol. 31, # 25 p. 3579 - 3582
反应条件
in DMF-d7 T=62°C; other temperatures and solvents; ΔH(excit.), ΔS(excit.), ΔG(excit.); KineticsThermodynamic data;
参考文献
Journal of Fluorine Chemistry, , vol. 80, # 2 p. 163 - 166
反应条件
2,4,6-trimethyl-pyridine; copper diacetate in N,N-dimethyl acetamide T=25°C; P=760.051 Torr; 16 h; Inert atmosphere;
参考文献
Xu, Jun; Luo, Dong-Fen; Xiao, Bin; Liu, Zhao-Jing; Gong, Tian-Jun; Fu, Yao; Liu, Lei
Chemical Communications, 2011 , vol. 47, # 14 p. 4300 - 4302
反应条件
in DMF-d7 T=62°C; other temperatures and solvents; ΔH(excit.), ΔS(excit.), ΔG(excit.); KineticsThermodynamic data;
参考文献
Journal of Fluorine Chemistry, , vol. 80, # 2 p. 163 - 166
反应条件
sodium iodide in N,N-dimethyl-formamide 72 h; Ambient temperature;
参考文献
Umemoto; Ishihara
Tetrahedron Letters, 1990 , vol. 31, # 25 p. 3579 - 3582
反应条件
2,4,6-trimethyl-pyridine; copper diacetate in N,N-dimethyl acetamide T=25°C; P=760.051 Torr; 16 h; Inert atmosphere;
参考文献
Xu, Jun; Luo, Dong-Fen; Xiao, Bin; Liu, Zhao-Jing; Gong, Tian-Jun; Fu, Yao; Liu, Lei
Chemical Communications, 2011 , vol. 47, # 14 p. 4300 - 4302
反应条件
2,4,6-trimethyl-pyridine; copper diacetate in N,N-dimethyl acetamide T=0°C; P=760.051 Torr; 16 h; Inert atmosphere;
参考文献
Xu, Jun; Luo, Dong-Fen; Xiao, Bin; Liu, Zhao-Jing; Gong, Tian-Jun; Fu, Yao; Liu, Lei
Chemical Communications, 2011 , vol. 47, # 14 p. 4300 - 4302